Plant fiber-based antibacterial material and preparation method thereof

A plant fiber and antibacterial material technology, applied in the field of plant fiber-based antibacterial materials and its preparation, can solve problems such as uneven dispersion, difficulty in forming bonds, and poor compatibility, and achieve excellent antibacterial properties

Inactive Publication Date: 2020-10-30
上海麟定生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although plant fiber materials have many advantages, plant fibers contain a large number of polar functional groups such as polar hydroxyl groups, which have poor compatibility with non-polar polymers, so it is difficult to form a good bond between plant fibers and the polymer matrix interface. At the same time, natural plant fiber molecules contain hydrogen bonds, which will gather together when heated, resulting in uneven dispersion in the matrix, thus affecting the comprehensive performance of composite materials
[0003] With the increasingly serious problem of environmental pollution, plant fibers have been widely used, but their physical and chemical properties need to be improved, especially in the fields of food, daily chemicals, sanitary materials and other fields with high hygiene requirements, plant fibers need to be improved before they can adapt special hygiene requirements

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Material ratio (by weight):

[0037] 100 parts of cane pulp fiber, 5 parts of corn starch, 1 part of chitosan, 0.2 part of 2,3-epoxypropyltrimethylammonium chloride, 0.01 part of sodium hydroxide, 0.1 part of acetic acid, 0.001 part of sodium tripolyphosphate , 1 part of sodium carboxymethylcellulose, 0.01 part of dopamine hydrochloride, 0.4 part of silane, 300 parts of water, and 10 parts of isopropanol.

[0038] A: Plant fiber modification

[0039] Put the sugarcane pulp fiber of the above components in hot water of 80-100 degrees, adjust the pH value to 6, add dopamine hydrochloride aqueous solution, silane and continue to grind and stir in the mixer for 30 minutes at a stirring speed of 1000-3000 rpm to obtain Cross-linked modified wet cane pulp.

[0040] B: chitosan modification

[0041] Dissolve the chitosan of the above components in the acetic acid solution, adjust the pH value to 5, add sodium tripolyphosphate, and stir at a medium speed of 75-80 degrees for...

Embodiment 2

[0049] Further, in order to simplify the production process, the materials prepared by the following method have slightly different functions, but still maintain good antibacterial effect and physical properties.

[0050] Material ratio (by weight):

[0051] 70 parts of cane pulp fiber, 30 parts of bamboo pulp fiber, 6 parts of corn starch, 1.5 parts of chitosan, 1 part of 2,3-epoxypropyltrimethylammonium chloride, 0.01 part of sodium hydroxide, 0.1 part of acetic acid, Sodium tripolyphosphate 0.01 part, water 300 parts, isopropanol 15 parts.

[0052] A: Physical modification of plant fibers

[0053] Put the sugarcane pulp fiber and bamboo pulp fiber of the above components in hot water of 80-90 degrees, adjust the pH value to 7, continue grinding and stirring in the mixer for 30 minutes, and the stirring speed is 2000-2500 rpm. A physically modified wet vegetable fiber pulp is obtained.

[0054] B: chitosan modification

[0055] The chitosan of the above components is dis...

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PUM

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Abstract

The invention discloses a plant fiber-based antibacterial material and a preparation method thereof. The plant fiber-based antibacterial material is prepared from the following substances in parts byweight: 95-100 parts of plant fibers, 2-20 parts of starch, 0.1-3 parts of chitosan, 1-10 parts of a modifying aid, 5-20 parts of isopropanol and 100-600 parts of water. The plant fiber-based antibacterial material has the characteristics of light weight, low cost, full degradation and excellent antibacterial performance, and can be widely applied to the field of direct contact packaging of foodsand other sanitary materials with higher sanitary requirements.

Description

technical field [0001] The invention belongs to the technical field of compound performance improvement of plant fiber materials, and in particular relates to a plant fiber-based antibacterial material and a preparation method thereof. Background technique [0002] As a renewable and environmentally friendly fiber material, plant fiber (straw, bagasse, hemp fiber, bamboo fiber, etc.) has abundant sources, low price, low processing cost, recyclable, degradable, light weight, high strength, corrosion resistance, etc. Features, can replace wood, plastic. Although plant fiber materials have many advantages, plant fibers contain a large number of polar functional groups such as polar hydroxyl groups, which have poor compatibility with non-polar polymers, so it is difficult to form a good bond between plant fibers and the polymer matrix interface. At the same time, natural plant fiber molecules contain hydrogen bonds, which will gather together when heated, resulting in uneven di...

Claims

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Application Information

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IPC IPC(8): C08L97/02C08L3/08C08L5/08C08L1/28C08B37/08C08B31/12C08H8/00
CPCC08B31/125C08B37/003C08H8/00C08L97/02C08L2201/06C08L2205/035C08L3/08C08L5/08C08L1/286
Inventor 邓小勇常庆何曙光
Owner 上海麟定生物科技有限公司
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