Method for preparing lily polysaccharide microcapsule
The technology of lily polysaccharide and microcapsule is applied in the field of food processing to achieve the effects of simple preparation process, enhanced immune function and prolonged action time.
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Embodiment 1
[0023] Take 1g of gelatin and 2g of gum arabic, dissolve them separately, and mix them evenly to prepare 300 mL of 1% mixed solution, then add 1.5 g of lily polysaccharide to the mixed solution, disperse at 1000 r / min for 3 minutes at high speed, and use 10% of Adjust the pH to 3.5 with glacial acetic acid, continue to stir at 40 °C for 20 minutes, then take it out, then cool it down to about 10 °C with an ice-water bath, adjust the pH to 6.0 with 10% sodium hydroxide, add 0.2 g of curing agent TGase, stir and solidify for 3 h, stand still and filter with suction to obtain the wet sac product, then spread the wet sac product on a petri dish, pre-cool at -20°C for 24 h, and then freeze-dry under 1 Pa pressure and vacuum condition, the time is not less than 24 h. h, to obtain solid microcapsules.
[0024] The average particle size of a newly prepared lily polysaccharide microcapsule is 132±11 μm, the embedding rate is 90.16%, and the content of lily polysaccharide in the lily po...
Embodiment 2
[0026] Take 1 g of gelatin and 1 g of gum arabic, dissolve them separately, and mix them evenly to prepare 200 mL of a 1% mixed solution, then add 2 g of lily polysaccharide to the mixed solution, disperse at a high speed for 3 min at 1000 r / min, and use 10% Adjust the pH to 4.0 with glacial acetic acid, continue to stir at 45°C for 30 minutes, take it out, then cool it down to about 10°C with an ice-water bath, adjust the pH to 6.0 with 10% sodium hydroxide, add 0.25g of curing agent TGase, stir and solidify After standing for 3 h and suctioning and filtering to obtain the wet sac product, spread the wet sac product on a petri dish, pre-cool at -20°C for 24 h, and then freeze-dry under 1 Pa pressure and vacuum condition, the time is not less than After 24 h, solid microcapsules were obtained.
[0027] The average particle size of a newly prepared lily polysaccharide microcapsule is 147±9μm, the embedding rate is 87.65, and the content of lily polysaccharide in the lily polysa...
Embodiment 3
[0029] Take 2 g of gelatin and 1 g of gum arabic, dissolve them separately, and mix them evenly to prepare a 300 mL 1% mixed solution, then add 6 g of lily polysaccharide to the mixed solution, disperse at a high speed of 1000 r / min for 3 min, and use Adjust the pH to 4.5 with 10% glacial acetic acid, take it out after continuing to stir at 50 °C for 40 min, then cool it down to about 10 °C with an ice-water bath, adjust the pH to 6.0 with 10% sodium hydroxide, add 0.6 g of curing agent TGase, Stir and solidify for 3 h, stand still and filter with suction to obtain the wet sac product, then spread the wet sac product on a petri dish, pre-cool at -20 °C for 24 h, and then freeze-dry it under 1 Pa pressure and vacuum condition for a certain time. Below 24 h, solid microcapsules were obtained.
[0030] The average particle size of a newly prepared lily polysaccharide microcapsule is 185±14 μm, the embedding rate is 80.15%, and the content of lily polysaccharide in the lily polysa...
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