UV orange-peel agent and orange-peel paint
An orange pattern agent and orange pattern technology, applied in the field of coatings, can solve the problems of difficult construction, poor pattern concave and convex feeling, etc., and achieve the effect of solving difficult construction, good effect and excellent adhesion.
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[0046] Orange grain agent preparation steps are as follows:
[0047] (1) 1mol of fluorine-containing monohydric alcohol (A) is added to the mixture containing 3wt% BF 3 In 1.1mol epichlorohydrin (B) in diethyl ether, heat to 45°C, react for 6h; stand still, and distill under reduced pressure at 40°C to obtain a ring-opening intermediate product; add 1.2mol sodium hydroxide to 1mol ring-opening intermediate product , stirred at 45°C for 4h, washed 3 times with deionized water, and obtained the ring-forming intermediate I (IR: 3509cm -1 : -OH disappears; 1253cm -1 :-C-F exists; 911cm -1 : presence of epoxy group; 1599cm -1 : C-O-C exists);
[0048] The BF 3 The dosage is 3wt% of the weight of A.
[0049] (2) Add 5 parts by weight of 2% aqueous sodium hydroxide solution to 1 part by weight of III, and stir at 40°C for 8 hours to obtain intermediate product II (IR: 1253cm -1 :-C-F exists; 1599cm -1 : C-O-C exists; 911cm -1 : Epoxy disappears; 3523cm -1 :-OH exists).
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