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White tea year discrimination method taking S-linalool and R/S-dihydroactinidiolide as markers

A dihydroactinolactone and discrimination method technology, applied in the field of white tea age discrimination, can solve problems such as temperature, humidity, light, psychological effects, restricting the healthy development of the white tea industry, and the degree of difference cannot be quantified, etc., to eliminate interference from human factors, Avoid waste of tea samples and judge the ideal effect

Active Publication Date: 2020-05-29
TEA RES INST CHINESE ACAD OF AGRI SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Sensory evaluation technology has high requirements for reviewers, who need to have sufficient review experience and keen sensory judgment ability, and cannot operate in batches; on the other hand, although Xinchen white tea has certain differences in flavor quality degree, but the degree of difference cannot be quantified, and it is difficult to accurately judge its storage year through sensory evaluation methods; in addition, the evaluation results are also deeply affected by external objective factors (such as temperature, humidity, light, psychological effects, etc.), so sensory evaluation techniques It has great limitations in distinguishing the age of white tea
This limitation has brought business opportunities to some unscrupulous traders. Driven by profit, they shoddy new white tea, or used low-year white tea to pretend to be old white tea, thereby reaping huge profits and seriously disrupting the market. order, which restricts the healthy development of the white tea industry

Method used

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  • White tea year discrimination method taking S-linalool and R/S-dihydroactinidiolide as markers
  • White tea year discrimination method taking S-linalool and R/S-dihydroactinidiolide as markers
  • White tea year discrimination method taking S-linalool and R/S-dihydroactinidiolide as markers

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Experimental program
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Effect test

Embodiment 1

[0031] (1) The ground white tea powder was weighed, and S-linalool, R-dihydroactinolide and S-dihydroactinolactone in white tea were extracted by headspace solid-phase microextraction. Three kinds of white tea samples, Baihaoyinzhen, Baimudan and Shoumei, were selected and tested respectively.

[0032] The method of headspace solid-phase microextraction is as follows: weigh 1g of ground white tea powder and 2g NaCl into a 20mL headspace extraction bottle and mix evenly, add 4ml of boiling water to brew, immediately screw the cap to mix well, and place the headspace bottle at 80 ºC Equilibrate in a metal incubator for 5 minutes, insert the headspace sampling handle equipped with aged DVB / CAR / PDMS (50 / 30μm, 2 cm) extraction fibers, and extract at a constant temperature of 80 ºC for 60 minutes. After the extraction is completed, immediately insert the GC- In the MS injection port, analyze for 5 min, collect data, and repeat 3 times in parallel for each sample.

[0033](2) The co...

Embodiment 2

[0063] Professionals are entrusted to purchase one representative sample of Baihao Yinzhen, Baimudan and Shoumei, and the year information is not disclosed to the test personnel in advance. According to the step (1) of the method of the present invention, the testers extracted S-linalool, R-dihydroactinolactone, and S-dihydroactinolactone in white tea with unknown storage years, and measured each white tea sample according to step (2). For the content of the above compounds, according to the flower color, substitute the corresponding content data into the linear equation described in step (3) to obtain the calculated value of each white tea year, combined with the reference error range in step (4), finally get the white tea storage year. Predictive value. In this embodiment, the predicted storage years and actual storage years of the 3 white tea samples are as follows:

[0064] Baihaoyinzhen: Theoretical predicted value: 3.2, predicted year range: 2.1-4.4, actual year: 4 year...

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Abstract

The invention discloses a white tea year discrimination method taking S-linalool and R / S-dihydroactinidiolide as markers and belongs to the technical field of tea discrimination. The method is characterized by comprising steps of takingpekoe silver needles, white peony and longevity eyebrows are used as white tea samples, establishing a linear regression equation of the contents of the S-linalool,the R-dihydroactinidiolide and the S-dihydroactinidiolide and the storage year, calculating an error reference value, substituting the measured contents of the S-linalool, the R-dihydroactinidiolideand the S-dihydroactinidiolide into the linear regression equation, and combining an error reference value to obtain an annual predicted value of the white tea sample. The method is advantaged in thatthe true judgment rate of the pekoe silver needle, the white peony and the longevity eyebrow tea in the actual year is high, and the three linear regression models are reliable.

Description

technical field [0001] The invention belongs to the technical field of tea identification, and in particular relates to a white tea age identification method using S-linalool and R / S-dihydroactinolactone as markers. Background technique [0002] White tea belongs to one of the six traditional Chinese teas. According to the difference in tenderness of fresh leaves, white tea can be divided into Baihao Yinzhen (single bud), Baimudan (one bud and one leaf or two leaves) and Shoumei (one bud More than three leaves or only leaves), and other varieties with different colors and flavors, have their own characteristics in flavor and quality, and have been loved and concerned by different consumer groups. White tea is resistant to storage and has similar storage value to black tea. White tea stored for a certain number of years not only has a unique charm, but also has more prominent health benefits. Aged white tea is known as "one-year tea, three-year medicine, and seven-year treas...

Claims

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Application Information

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IPC IPC(8): G01N30/88G01N30/06
CPCG01N30/88G01N30/06G01N2030/062
Inventor 朱荫林智严寒吕海鹏张悦戴伟东郭丽施江谭俊峰彭群华
Owner TEA RES INST CHINESE ACAD OF AGRI SCI
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