White tea year discrimination method taking S-linalool and R/S-dihydroactinidiolide as markers
A dihydroactinolactone and discrimination method technology, applied in the field of white tea age discrimination, can solve problems such as temperature, humidity, light, psychological effects, restricting the healthy development of the white tea industry, and the degree of difference cannot be quantified, etc., to eliminate interference from human factors, Avoid waste of tea samples and judge the ideal effect
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Embodiment 1
[0031] (1) The ground white tea powder was weighed, and S-linalool, R-dihydroactinolide and S-dihydroactinolactone in white tea were extracted by headspace solid-phase microextraction. Three kinds of white tea samples, Baihaoyinzhen, Baimudan and Shoumei, were selected and tested respectively.
[0032] The method of headspace solid-phase microextraction is as follows: weigh 1g of ground white tea powder and 2g NaCl into a 20mL headspace extraction bottle and mix evenly, add 4ml of boiling water to brew, immediately screw the cap to mix well, and place the headspace bottle at 80 ºC Equilibrate in a metal incubator for 5 minutes, insert the headspace sampling handle equipped with aged DVB / CAR / PDMS (50 / 30μm, 2 cm) extraction fibers, and extract at a constant temperature of 80 ºC for 60 minutes. After the extraction is completed, immediately insert the GC- In the MS injection port, analyze for 5 min, collect data, and repeat 3 times in parallel for each sample.
[0033](2) The co...
Embodiment 2
[0063] Professionals are entrusted to purchase one representative sample of Baihao Yinzhen, Baimudan and Shoumei, and the year information is not disclosed to the test personnel in advance. According to the step (1) of the method of the present invention, the testers extracted S-linalool, R-dihydroactinolactone, and S-dihydroactinolactone in white tea with unknown storage years, and measured each white tea sample according to step (2). For the content of the above compounds, according to the flower color, substitute the corresponding content data into the linear equation described in step (3) to obtain the calculated value of each white tea year, combined with the reference error range in step (4), finally get the white tea storage year. Predictive value. In this embodiment, the predicted storage years and actual storage years of the 3 white tea samples are as follows:
[0064] Baihaoyinzhen: Theoretical predicted value: 3.2, predicted year range: 2.1-4.4, actual year: 4 year...
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