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Charging container for combustion, charging method of charging container for combustion and synthesis method of high alpha-phase silicon nitride

A charging container and a charging technology are applied to a charging container for combustion and a charging method thereof, and the synthesis field of high-alpha phase silicon nitride, which can solve the problems of waste, labor and time, and achieve the purpose of recycling powder. The effect of less quantity, reduced picking workload, and high combustion efficiency

Pending Publication Date: 2020-05-19
XINJIANG JINGSHUO NEW MATERIALS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Patent CN200410029809.3 puts the raw material powder into a porous graphite crucible for combustion synthesis reaction, which takes a lot of manpower and time in the selection of the output powder, resulting in unnecessary waste

Method used

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  • Charging container for combustion, charging method of charging container for combustion and synthesis method of high alpha-phase silicon nitride
  • Charging container for combustion, charging method of charging container for combustion and synthesis method of high alpha-phase silicon nitride
  • Charging container for combustion, charging method of charging container for combustion and synthesis method of high alpha-phase silicon nitride

Examples

Experimental program
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Embodiment 1

[0035] This embodiment provides a charging container for combustion, including: a charging boat for charging, the charging boat is a hollow structure with an open top, and the charging container for combustion also includes: thermal insulation material, and a hollow structure for the charging boat The inside is filled with breathable thermal insulation material, or the surface of the charging boat is provided with breathable thermal insulation material.

[0036] This embodiment provides a charging method using the above-mentioned charging container for combustion, comprising the following steps:

[0037] 1) Fill the material to be burned in the above-mentioned charging container;

[0038] 2) Select the ignition area in the charging container, dig out the materials to be burned in the ignition area, add an ignition wire in the ignition area, then add the ignition powder that is not filled with the ignition area in the ignition area, and then add the ignition powder in the ignit...

Embodiment 2

[0044] Such as Figure 1~3 As shown, the present embodiment provides a charging container for combustion, including: a charging boat 1 for charging, the charging boat 1 is a hollow structure with an open top, and the charging container for combustion also includes: an insulating material 2, The hollow structure of the charging boat 1 is filled with a breathable thermal insulation material 2 , or the surface of the charging boat 1 is provided with a breathable thermal insulation material 2 .

[0045] Such as figure 1 As shown, it should be noted that the hollow structure of the charging boat 1 in this embodiment is a hollow structure formed by connecting strip rods 3 arranged parallel to each other through connecting rods 8 .

[0046] It should be noted that, in this embodiment, the gap between two adjacent strip bars 3 parallel to each other is 25mm.

[0047] It should be noted that the porosity of the thermal insulation material 2 in this embodiment is 30-60%.

[0048] Suc...

Embodiment 3

[0067] The present embodiment provides a kind of charging container for combustion, and the difference in embodiment 2 is:

[0068] It should be noted that, in this embodiment, the gap between two adjacent bar-shaped bars parallel to each other is 5 mm.

[0069] It should be noted that the porosity of the thermal insulation material in this embodiment is 30-60%.

[0070] It should be noted that the thermal insulation material in this embodiment is alumina fiber felt.

[0071] It should be noted that the material of the charging boat in this embodiment is 316 stainless steel.

[0072] This embodiment also provides a charging method using the above-mentioned charging container for combustion, which differs from the charging method in Embodiment 2 as follows:

[0073] The composite powder described in step 2) is obtained by mixing the ignition powder dug out from the ignition area with 1 / 3 of its weight silicon powder.

[0074] It should be noted that the ignition powder in th...

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Abstract

The invention discloses a charging container for combustion, a charging method of the charging container for the combustion and a synthesis method of high alpha-phase silicon nitride. The charging container for the combustion comprises a charging boat for charging and is characterized in that the charging boat is a hollow structure with an opening at the top, the charging container for the combustion further comprises heat-insulating materials, and the hollow structure of the charging boat is internally filled with air-permeable heat-insulating materials; or the surface of the charging boat isprovided with the air-permeable heat-insulating materials. According to the charging container for the combustion and the charging method of the charging container for the combustion, the ignition success rate is ensured to reach 99% or above, the combustion efficiency is high, the smooth progress of combustion is guaranteed, it is ensured that no burning phenomenon occurs in the spreading process during combustion, the amount of recycled powder is small, and the picking workload of unburnt materials after combustion is reduced, meanwhile, the combustion time and the post-end discharge powdermaterial treatment period are greatly shortened, dust pollution in the prior art operation process is avoided, and the production efficiency is improved.

Description

technical field [0001] The invention belongs to the technical field of combustion charging, and in particular relates to a combustion charging container, a charging method thereof, and a synthesis method of high-α-phase silicon nitride. Background technique [0002] As an emerging powder material, silicon nitride is widely used in photovoltaics, machinery, chemicals, semiconductors, ceramics and other industrial fields because of its good mechanical strength, chemical properties, thermal shock resistance and electrical insulation. In the known silicon nitride production technology, the nitridation time of the direct nitridation method is long and the power consumption is high. To produce high-quality products requires not only fine control of the process, but also strict requirements on equipment. But its production efficiency is low, and the silicon nitride powder produced at the same time is conventional low-quality ceramic powder; the ammonolysis method uses silicon tetra...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): F27D3/00F27D5/00
CPCF27D3/0025F27D3/0084F27D5/0068
Inventor 张吉武黄彬宗鑫梁立刚卢宏韬邵亮亮
Owner XINJIANG JINGSHUO NEW MATERIALS CO LTD
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