Preparation method for self-active lithium titanate material
A technology of self-activating lithium titanate and lithium acetate, applied in titanate, alkali metal titanate, chemical instruments and methods, etc., can solve the problems of poor conductivity of lithium titanate, and improve the conductivity and activity Effect
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preparation example Construction
[0022] A preparation method of self-active lithium titanate material, comprising the steps of:
[0023] Step 1, adding lithium acetate to absolute ethanol and stirring evenly for 1-3 hours to obtain a lithium alcohol solution;
[0024] Step 2, adding titanium monoxide powder into the lithium alcohol solution for low-temperature ultrasonication for 2-4 hours to obtain a mixed suspension;
[0025] Step 3, evenly spray the mixed suspension into the sealed reaction kettle, let it stand at a constant temperature for 1-2 hours, release the pressure and cool down to obtain coated titanium monoxide particles;
[0026] Step 4, adding the coated titanium monoxide particles into the mold for constant temperature and pressure reaction for 2-4 hours to obtain the primary lithium titanate plate;
[0027] Step 5: Soak the primary plate of lithium titanate in tetrabutyl titanate and sonicate at low temperature for 3-5 hours, then squeeze and react for 2-4 hours in a humid environment, and si...
Embodiment 1
[0036] A preparation method of self-active lithium titanate material, comprising the steps of:
[0037] Step 1, adding lithium acetate to absolute ethanol and stirring evenly for 1 hour to obtain a lithium alcohol solution;
[0038] Step 2, adding titanium monoxide powder into the lithium alcohol solution for low-temperature ultrasonication for 2 hours to obtain a mixed suspension;
[0039] Step 3, evenly spray the mixed suspension into the sealed reaction kettle, let it stand at a constant temperature for 1 hour, release the pressure and cool down to obtain coated titanium monoxide particles;
[0040] Step 4, adding the coated titanium monoxide particles into the mold for constant temperature and pressure reaction for 2 hours to obtain a primary lithium titanate plate;
[0041] Step 5: Soak the primary plate of lithium titanate in tetrabutyl titanate for low-temperature ultrasonication for 3 hours, then squeeze and react for 2 hours in a humid environment, and sinter to obta...
Embodiment 2
[0051] A preparation method of self-active lithium titanate material, comprising the steps of:
[0052] Step 1, adding lithium acetate to absolute ethanol and stirring evenly for 3 hours to obtain a lithium alcohol solution;
[0053] Step 2, adding titanium monoxide powder into the lithium alcohol solution for low-temperature ultrasonication for 4 hours to obtain a mixed suspension;
[0054] Step 3, evenly spray the mixed suspension into the sealed reaction kettle, let it stand at a constant temperature for 2 hours, release the pressure and cool down to obtain coated titanium monoxide particles;
[0055] Step 4, adding the coated titanium monoxide particles into the mold for a constant temperature and pressure reaction for 4 hours to obtain a primary lithium titanate plate;
[0056] Step 5: Soak the primary plate of lithium titanate in tetrabutyl titanate for 5 hours of low-temperature ultrasonication, then squeeze and react for 4 hours in a humid environment, and sinter to o...
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