Preparation method of lithium titanate material
A technology of lithium titanate and lithium acetate, applied in titanate, alkali metal titanate, chemical instruments and methods, etc., can solve problems such as poor electrical conductivity, and achieve the effect of improving electrical conductivity and improving mobility
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[0024] A preparation method of lithium titanate material, comprising the steps of:
[0025] Step 1, adding tetrabutyl titanate into absolute ethanol and stirring evenly to form a titanium alcohol solution;
[0026] Step 2, adding lithium acetate to the titanic acid solution and stirring evenly to form a mixed solution;
[0027] Step 3, adding titanium monoxide powder to the mixed solution and ultrasonically ultrasonicating at low temperature for 1-2 hours to obtain a suspension;
[0028] Step 4, spray the suspension into a constant temperature reaction kettle, seal and deposit, release pressure and cool to obtain coated titanium monoxide particles;
[0029] Step 5, put the coated titanium monoxide particles into a sealed reaction kettle and let it stand at constant pressure for 1-3 hours, then pass in water vapor for a sealed pressurized reaction for 2-3 hours, and seal and sinter to obtain lithium titanate particles after pressure release.
[0030] The concentration of n-bu...
Embodiment 1
[0041] A preparation method of lithium titanate material, comprising the steps of:
[0042] Step 1, adding tetrabutyl titanate to absolute ethanol and stirring evenly to form a titanium alcohol solution; the concentration of n-butyl titanate in absolute ethanol is 100g / L, and the stirring speed is 1000r / m;
[0043] Step 2, adding lithium acetate into the titanic acid solution and stirring evenly to form a mixed solution; the amount of lithium acetate added is 110% of the molar weight of n-butyl titanate, and the stirring speed is 1500r / min;
[0044] Step 3: Add titanium monoxide powder to the mixed solution for low-temperature ultrasonication for 1 hour to obtain a suspension; titanium monoxide powder is a micron-sized powder with a particle size of 10 μm; low-temperature ultrasonication adopts high-frequency gap ultrasonication, and the low temperature is 5°C , the ultrasonic frequency is 60kHz, the single ultrasonic time is 5s, and the ultrasonic interval is 10s;
[0045] S...
Embodiment 2
[0049] A preparation method of lithium titanate material, comprising the steps of:
[0050] Step 1, adding tetrabutyl titanate to absolute ethanol and stirring evenly to form a titanium alcohol solution; the concentration of n-butyl titanate in absolute ethanol is 200g / L, and the stirring speed is 2000r / m;
[0051] Step 2, adding lithium acetate to the titanic acid solution and stirring evenly to form a mixed solution; the amount of lithium acetate added is 140% of the molar weight of n-butyl titanate, and the stirring speed is 2500r / min;
[0052] Step 3: Add titanium monoxide powder to the mixed solution for low-temperature ultrasonication for 2 hours to obtain a suspension; titanium monoxide powder is a micron-sized powder with a particle size of 500 μm; low-temperature ultrasonication adopts high-frequency gap ultrasonication, and the low temperature is 10°C , the ultrasonic frequency is 90kHz, the single ultrasonic time is 10s, and the ultrasonic interval is 20s;
[0053]...
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