A kind of light stabilizer and its preparation method and application
A light stabilizer and solvent technology, applied in the field of light stabilizer and its preparation, to achieve long-term light stability and physical and mechanical performance stability, excellent physical and mechanical performance, and the effect of weakening the catalytic effect
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Embodiment 1
[0039] Preparation of Light Stabilizer A1:
[0040] In a four-necked flask equipped with a thermometer, add II, 105g of 1,1,6,6-tetramethylpiperidinamine, 53g of 3-(2,3-epoxypropoxy)propyltrimethoxysilane, Dissolve it in 350g of toluene solvent, install a condenser, start the stirrer, and raise the temperature to 65°C for 4 hours in a water bath. After the ring-opening addition reaction, the organic solvent and unreacted small molecule intermediates were distilled off under reduced pressure to obtain the target product with a yield of 94%. According to infrared characterization, the obtained product is at 910cm -1 The characteristic peak of the epoxy group at around 3300cm disappears, while at 3300cm -1 There are obvious alcoholic hydroxyl peaks at the left and right.
Embodiment 2
[0042] Preparation of Light Stabilizer A2:
[0043] In a four-necked flask equipped with a thermometer, add II, 150g of 1,1,6,6-tetramethylpiperidinamine, 120g of 3-(2,3-epoxypropoxy)propyltriethoxysilane , dissolved in 350g of ethanol solvent, fitted with a condenser, started the agitator, and heated to 25°C for 6 hours in a water bath. After the ring-opening addition reaction, the organic solvent and unreacted small molecule intermediates were distilled off under reduced pressure to obtain the target product with a yield of 96%.
Embodiment 3
[0045] The preparation of light stabilizer A3:
[0046] In a four-necked flask equipped with a thermometer, add 150g of II, 1,1,6,6-tetramethylpiperidinamine, 3-(2,3-epoxypropoxy)propyldimethoxymethyl 150g of silane was dissolved in 600g of petroleum ether solvent, a condenser was installed, the stirrer was started, and the temperature was raised to 90°C for 9 hours in a water bath. After the ring-opening addition reaction, the organic solvent and unreacted small molecule intermediates were distilled off under reduced pressure to obtain the target product with a yield of 93%.
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