A kind of X-ray detector based on perovskite single crystal particle composite film and its preparation method
A technology of ray detectors and single crystal particles, which is applied in the field of X-ray detectors based on perovskite single crystal particle composite films and its preparation, can solve the problem of large dark current, low sensitivity, and slow response of X-ray detectors. problems, to achieve good application prospects, fast response, low dark current and low noise
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Embodiment 1
[0039] A preparation method based on perovskite single crystal particle composite film X-ray detector, comprising the following steps:
[0040] 1) Methylamine lead bromide salt (CH 3 NH 3 PbBr 3 ) perovskite single crystal, the solution of methylamine lead bromide salt was fully dissolved at 40°C to obtain a saturated solution, and after filtration, it was continuously heated at 100°C for 12 hours to grow a single crystal of methylamine lead bromide salt perovskite. The single crystal particle size of granular perovskite is 1.5cm;
[0041] 2) After drying the methylamine lead bromide perovskite single crystal described in step 1), perform mechanical crushing and sieving to obtain methylamine lead bromide perovskite single crystal particles, and dry it in a vacuum oven at 60°C for 24 Hours, crushing using a ball mill, sieving using a vibrating sieve, and the particle size of the single crystal particles obtained after crushing and sieving is 30-40 μm;
[0042]3) The mixed s...
Embodiment 2
[0056] A preparation method based on perovskite single crystal particle composite film X-ray detector, comprising the following steps:
[0057] 1) Methylamine lead bromide (CH 3 NH 3 PbBr 3 ) perovskite single crystal, fully dissolve the solution of methylamine lead bromide salt at 40°C to obtain a saturated solution, filter and continue heating at 70°C for 12 hours to slowly evaporate the solvent to obtain methylamine lead bromide salt perovskite single crystal , in which the single crystal grain size of large-grained perovskite is 0.5cm;
[0058] 2) After drying the methylamine lead bromide perovskite single crystal described in step 1), perform mechanical crushing and sieving to obtain methylamine lead bromide perovskite single crystal particles, and dry it in a vacuum oven at 60°C for 24 Hours, crushing using a ball mill, sieving using a vibrating sieve, and the particle size of the single crystal particles obtained after crushing and sieving is 40-50 μm;
[0059] 3) T...
Embodiment 3
[0066] A preparation method based on perovskite single crystal particle composite film X-ray detector, comprising the following steps:
[0067] 1) Methylamine lead bromide salt (CH 3 NH 3 PbBr 3 ) perovskite single crystal, the solution of methylamine lead bromide salt was fully dissolved at 40°C to obtain a saturated solution, and after filtration, it was continuously heated at 120°C for 14 hours to grow a single crystal of methylamine lead bromide salt perovskite. The single crystal particle size of granular perovskite is 1cm;
[0068] 2) After drying the methylamine lead bromide perovskite single crystal described in step 1), perform mechanical crushing and sieving to obtain methylamine lead bromide perovskite single crystal particles, and dry it in a vacuum oven at 60°C for 24 Hours, crushing using a ball mill, sieving using a vibrating sieve, and the particle size of the single crystal particles obtained after crushing and sieving is 40-50 μm;
[0069] 3) The mixed su...
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