Preparation method of cranberry extract
A technology of extract and cranberry, which is applied in the field of preparation of cranberry extract, can solve problems such as potential safety hazards and decreased lung function, and achieve the effects of improving stability, high utilization of raw materials, and improving biological activity
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Embodiment 1
[0030] The preparation method of the cranberry extract of the present embodiment comprises the following steps:
[0031] A, extraction, concentration: 50.5kg (moisture content 76.34wt%) of broken cranberry fresh fruit is placed in the extraction tank, and acidic ethanol solution I [acidic ethanol solution I] that is equivalent to 10 times the volume of cranberry fresh fruit raw material is added The volume concentration of ethanol in the medium is 85%. The acids are mixed organic acids. The mixed organic acid is a mixed acid of citric acid, malic acid and quinic acid (molar ratio 1:1:2). In the acidic ethanol solution I, the total molar concentration of the mixed organic acids is 0.01mol / L], reflux extraction at 85°C for 3 times, each reflux extraction for 0.5 hours, the resulting extract was concentrated under reduced pressure at 70°C, and the alcohol was recovered to obtain Concentrate;
[0032] B, centrifugation: the concentrated solution obtained in step A is separated ...
Embodiment 2
[0036] The preparation method of the cranberry extract of the present embodiment comprises the following steps:
[0037] A, extract, concentrate: the cranberry fresh fruit 51.4kg (moisture: 77.52%) of fragmentation is dropped in the extracting tank, add the acid ethanol solution I [acid ethanol that is equivalent to cranberry fresh fruit raw material volume 12,10,8 times respectively The volume concentration of ethanol in solution I is 75%, and the acid therein is a mixed organic acid. The mixed organic acids are citric acid, malic acid, acetic acid, and benzoic acid, the molar ratio of which is 1:1:2:2, and the total molar concentration of the mixed organic acids in the acidic ethanol solution is 0.015mol / L], reflux extraction at 90°C 3 times, the extraction time was 1.0 hour, 0.5 hour and 0.5 hour respectively. Concentrate the obtained extract under reduced pressure at 70°C, recover the alcohol, and obtain the concentrate;
[0038] B, centrifugation: the concentrate obtain...
Embodiment 3
[0042] The preparation method of the cranberry extract of the present embodiment comprises the following steps:
[0043] A, extract, concentrate: the cranberry fresh fruit 49.8kg (moisture: 80.06%) of fragmentation is placed in the extraction tank, add the acidic ethanol solution I that is equivalent to cranberry fresh fruit raw material volume 10,10,8 times respectively[ The volume concentration of ethanol in the acidic ethanol solution I is 65%. The acids are mixed organic acids. The mixed organic acids are citric acid, malic acid, quinic acid, acetic acid and benzoic acid, and their molar ratio is 1:2:2:1:1. In the acidic ethanol solution, the total molar concentration of the mixed organic acids is 0.02mol / L ], reflux extraction at 95°C for 3 times, each extraction time was 1.0 hour / time. Concentrate the obtained extract under reduced pressure at 70°C, recover the alcohol, and obtain the concentrate;
[0044] B, centrifugation: the concentrated solution obtained in step ...
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