Preparation method of transparent fireproof gel and composite fireproof glass
A gel and transparent technology, applied in the direction of parallel glass structures, windows/doors, building components, etc., can solve the problems of low water glass modulus, poor dispersion stability, viscosity increase, etc., to avoid indirect losses and improve fire resistance , the effect of low overall cost
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Embodiment 1
[0045] The raw materials were prepared according to the components and dosages of Example 1 shown in Table 1, and the thickness of the glass was 5mm. Follow the steps below to prepare composite fireproof glass.
[0046] 1) Add 15 parts by weight of a stabilizer to 100 parts of alkaline silica sol, mix at 1000 rpm for 30 minutes, continue stirring while raising the temperature to 80°C for evaporation and concentration, when the evaporation amount is alkaline silica sol 5% of the parts (ie 5 parts by weight), cooled to room temperature, and stirred at 1000 rpm for 2 hours to obtain an inorganic dispersion;
[0047] 2) Add 60 parts by weight of an aqueous solution of potassium hydroxide with a mass fraction of 50% to the inorganic dispersion prepared above, stir at room temperature at 1000 rpm for 10 min, heat up to 50° C. and stir for 30 min in a vacuum state, After cooling, the transparent fireproof gel precursor liquid is prepared, and it is used for subsequent use;
[0048]...
Embodiment 4
[0055] The dispersant in Example 4 and Example 5 is γ-aminopropyltriethoxysilane.
Embodiment 6
[0056] In Example 6 and Example 7, the dispersant is gamma-glycidyl etheroxypropyl trimethoxysilane, and the flame retardant is sodium phosphate. In Example 8-11, the dispersant is methyltrimethoxysilane, and the flame retardant is Guanidine phosphate, the carbon forming agent is pentaerythritol.
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