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Magnetic control nano-forming micromechanical device and three-dimensional fiber forming method

A nano-forming and micro-mechanical technology, applied in the field of spinning and forming, can solve the problems of messy fiber arrangement, long time-consuming, high conductivity of polymer solution, etc.

Active Publication Date: 2019-12-13
SICHUAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the electrospinning method still has the following shortcomings: (1) In order to generate sufficient electrostatic force, a high-voltage electrostatic field of tens of thousands of volts or even hundreds of thousands of volts is required, which not only greatly increases the cost of industrial production, but also poses serious safety hazards (2) The conductivity of the polymer solution used in spinning requires high conductivity and requires post-maintenance, resulting in high cost and long time-consuming; (3) the Taylor cone-shaped droplets formed in the spinning process not only The yield of nanofibers is low, and the prepared nanofibers are difficult to be used in practical applications due to the disordered arrangement; (4) The prepared nanofibers exist in the form of non-woven fabrics, and the fiber arrangement is very messy, which restricts its popularization and application
[0004] It can be seen that the molding problems based on micron-scale and nano-scale components are still not well resolved, and it is even more difficult to effectively apply them in the fields of biomedicine and chemistry.

Method used

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  • Magnetic control nano-forming micromechanical device and three-dimensional fiber forming method
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  • Magnetic control nano-forming micromechanical device and three-dimensional fiber forming method

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Embodiment 1

[0056] Based on the characteristics of magnetic fluid, this embodiment provides a magnetically controlled nano-molded micromechanical device, such as figure 1 and figure 2 As shown, it includes a magnetic fluid preparation device 1 for generating magnetic fluid, a three-dimensional control nano-table 2 for fixing the magnetic fluid preparation device, a working platform 3 below the magnetic fluid preparation device and a strong magnet 4 below the working platform . The present embodiment strong magnet adopts neodymium iron boron strong magnet.

[0057] Such as image 3 and Figure 4 As shown, the magnetic fluid preparation device 1 used in this embodiment includes a magnetic fluid generating mechanism 11 , a pushing mechanism 12 and a fixing mechanism 13 . The magnetic fluid generating mechanism 11 includes a container chamber 111, a nozzle 113 configured with a solenoid valve 112 is installed at the liquid outlet position of the container chamber, and the container chamb...

Embodiment 2

[0081] This embodiment provides another spinning three-dimensional molding method. The spinning raw material for this example is obtained by uniformly mixing citrate-stabilized magnetic nanoparticle dispersion and polyethylene oxide (PEO) solution with a concentration of 14 wt% in a volume ratio of 1:1.

[0082] Magnetic nanoparticles are prepared by conventional co-precipitation method (see A.Tokarev, W.–k., I.Sevonkaev, D.Goia, K.G.Kornev, Soft Matter 2014,10,1917, etc.). During the synthesis process, under stirring conditions, 1.625g (8mmol) FeCl 2 4H 2 O and 4.43g (16mmol) FeCl 3 ·6H 2 O was dissolved in 190 mL of water. 10 mL of aqueous ammonia at a concentration of 25 wt% was added to the solution, which resulted in the formation of a black magnetite precipitate. After stirring for 10 minutes, the precipitate was magnetically separated from the solution, and the precipitate was washed three times with deionized (DI) water to obtain magnetic nanoparticles.

[0083] ...

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Abstract

The invention discloses a magnetic control nano-forming micromechanical device and a three-dimensional fiber forming method. The magnetic control nano-forming micromechanical device comprises a magnetic fluid preparation device for generating magnetic fluid, a three-dimensional control nano-stage for fixing the magnetic fluid preparation device, a working platform positioned below the magnetic fluid preparation device and a strong magnet positioned below the working platform. According to the magnetic control nano-forming micromechanical device and the spinning three-dimensional forming method, based on the magnetic spinning forming principle, the magnetic fluid extruded from a feeding nozzle of the magnetic fluid preparation device forms a liquid bridge under the action of the magnetic field of the strong magnet, and the liquid bridge is solidified to form nanofiber fibers. As the relative position between the feeding nozzle of the magnetic fluid preparation device and the strong magnet can be accurately controlled via the three-dimensional control nano-stage, three-dimensional fibers meeting the set arrangement requirements can be prepared based on the set forming track. The device has the characteristics of being easy to operate and high in control precision, can meet requirements of industrial quantitative production, and has a good application prospect in the field.

Description

technical field [0001] The invention belongs to the technical field of spinning and forming, and relates to a magnetically controlled nano-forming micromechanical device and a spinning three-dimensional forming method based on magnetic principles for spinning and forming. Background technique [0002] Rapid prototyping (RP) technology is an advanced manufacturing technology developed in the 1990s. It is a key common technology for the development of new products for manufacturing companies. Improving product competitiveness has a positive role in promoting. The existing working principles include 3DP technology, SLA stereolithography technology, SLS selective laser sintering technology, DLP laser molding technology, FDM fusion lamination molding technology principle, etc., among which the more mature technology is the electrospinning nanofiber based on 3DP technology Preparation Process. [0003] Electrospinning is a spinning method that uses electrostatic force to produce...

Claims

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Application Information

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IPC IPC(8): B29C64/20B29C64/112B29C64/314B33Y30/00B33Y10/00B33Y40/00
CPCB29C64/112B29C64/20B29C64/314B33Y10/00B33Y30/00B33Y40/00
Inventor 张凯赵武成佳庆陈领郭鑫于淼王洋李骏王晓明
Owner SICHUAN UNIV
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