Preparation and use method of high hardness moisture-proof terrace hardener
A hardening agent, high hardness technology, applied in the direction of coating, can solve the problems of difficult construction and cumbersome process, and achieve the effect of hardness improvement and excellent stability
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Embodiment 1
[0025] At a temperature of 0°C and under stirring conditions of 100 r / min, add 40 parts by mass of methyl orthosilicate to 40 parts by mass of ethanol and stir for 10 minutes, then add 5 parts by mass of aqueous hydrochloric acid with a molar concentration of 2M in 20 times, Each interval is 20min, and then stirred for 10hr; under the stirring condition of 100r / min, add 40 mass parts of nano-silica sol and stir for 30min, and age at 25°C for 2 days; add 70 mass parts of the aged composite sol Continue to add 10 parts by mass of isopropanol to the nanometer floor hardener; after stirring for 30 minutes, add a hardening accelerator accounting for 3‰ of the mass ratio to the mixture, and stir for another 30 minutes to finally obtain a high hardness moisture-proof floor hardener .
[0026] The using method of this high hardness moisture-proof floor hardening agent is as follows (following embodiment and comparative example are all identical):
[0027] After polishing the self-lev...
Embodiment 2
[0029] At a temperature of 5°C, under stirring conditions of 100 r / min, 45 parts by mass of methyl orthosilicate was added to 40 parts by mass of ethanol and stirred for 10 minutes, and 7 parts by mass of aqueous hydrochloric acid with a molar concentration of 2M was added in 20 times. Each interval is 20min, and then stirred for 10hr; under the stirring condition of 200r / min, add 50 mass parts of nano-silica sol and stir for 30min, and age at 25°C for 2 days; add 60 mass parts of the aged composite sol Continue to add 10 parts by mass of isopropanol to the nanometer floor hardener; after stirring for 30 minutes, add a hardening accelerator accounting for 4‰ of the mass ratio to the mixture, and stir for another 30 minutes to finally obtain a high hardness moisture-proof floor hardener .
Embodiment 3
[0031] At a temperature of 10°C and under stirring conditions of 100 r / min, 50 parts by mass of methyl orthosilicate was added to 40 parts by mass of ethanol and stirred for 10 minutes, and 10 parts by mass of an aqueous hydrochloric acid solution with a molar concentration of 2M was added in 20 times. Each interval is 20min, and then stirred for 10hr; under the stirring condition of 150r / min, add 60 mass parts of nano-silica sol and stir for 30min, and age at 20°C for 2 days; add 50 mass parts of the aged composite sol Continue to add 10 parts by mass of isopropanol to the nanometer floor hardener; after stirring for 30 minutes, add a hardening accelerator accounting for 5‰ of its mass ratio to the mixture, and stir for another 30 minutes to finally obtain a high hardness moisture-proof floor hardener .
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