A kind of graphene mask cloth and preparation method thereof
A graphene surface, olefin mask technology, applied in chemical instruments and methods, pharmaceutical formulations, rayon manufacturing and other directions, can solve the problems of poor bacteriostatic effect, dust, weak adsorption capacity of cosmetics, etc., to reduce blocking and promote cross-linking. , Improve the effect of microcirculation
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[0039] A kind of preparation method of graphene mask cloth, comprises the steps:
[0040] (1) Take corncobs and grind them through a 100-mesh sieve in a grinder, collect the sieved matter and add a sodium carbonate solution with a mass fraction of 12% at a mass ratio of 1:6-10, and stir at 30-45°C at 400-700r / min Mix for 30 to 55 minutes, filter, take the filter cake and wash it with water for 2 to 4 times, take the filter cake and add HCl solution with a mass fraction of 15% according to the mass ratio of 1:7 to 12, mix and stir for 30 to 50 minutes, filter with suction, collect the filter residue in a microwave oven Treat with 400W power for 4-7 minutes to get the processed product. In terms of parts by mass, take 20-30 parts of processed product and 1-3 parts of FeCl 2 , 1 to 3 parts of FeCl 3, 2 to 5 parts of potassium chloride, 150 to 200 parts of water are mixed in a reactor, stirred at 40 to 55 °C at 350 to 550 r / min for 1 to 3 hours, and then ultrasonically treated at...
Embodiment 1
[0050] A kind of preparation method of graphene mask cloth, comprises the steps:
[0051] (1) Take corncobs and grind them through a 100-mesh sieve in a pulverizer, collect the sieved matter and add a sodium carbonate solution with a mass fraction of 12% at a mass ratio of 1:6, stir and mix at 30°C at 400r / min for 30min, filter, and take Wash the filter cake twice with water, take the filter cake and add HCl solution with a mass fraction of 15% according to the mass ratio of 1:7, mix and stir for 30 minutes, filter with suction, collect the filter residue and treat it in a microwave oven with a power of 400W for 4 minutes to obtain the processed product, calculated in parts by mass , take 20 parts of treatment, 1 part of FeCl 2 , 1 part of FeCl 3 , 2 parts of potassium chloride, and 150 parts of water were mixed in a reactor, stirred at 40° C. at 350 r / min for 1 hour, and then ultrasonically treated at a frequency of 45 kHz for 12 minutes to obtain an ultrasonically treated m...
Embodiment 2
[0061] A kind of preparation method of graphene mask cloth, comprises the steps:
[0062] (1) Take corncobs and grind them through a 100-mesh sieve in a pulverizer, collect the sieved matter and add a sodium carbonate solution with a mass fraction of 12% at a mass ratio of 1:10, stir and mix at 45°C at 700r / min for 55min, filter, and take Wash the filter cake with water for 4 times, take the filter cake and add HCl solution with a mass fraction of 15% according to the mass ratio of 1:12, mix and stir for 50 minutes, filter with suction, collect the filter residue and treat it in a microwave oven with a power of 400W for 7 minutes to obtain the treated product, calculated in parts by mass , take 30 parts of treatment, 3 parts of FeCl 2 , 3 parts FeCl 3 , 5 parts of potassium chloride, and 200 parts of water were mixed in a reactor, stirred at 55° C. for 3 hours at 550 r / min, and then ultrasonically treated at a frequency of 55 kHz for 20 minutes to obtain an ultrasonically tre...
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