Gas sealing device for continuous carbonization furnace

A carbonization furnace and gas sealing technology, applied in the chemical characteristics of fibers, textiles and papermaking, etc., can solve the problems of oxidation, affecting the performance of mesophase pitch-based carbon fibers, and the high cost of carbon fibers, and achieve the effect of avoiding eddy currents

Active Publication Date: 2019-09-27
湖南纪璟新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

On the one hand, since the strength of pre-oxidized filaments is only 10-50MPa, it is impossible to realize engineering production through large-scale continuous drawing; stay high
If continuous carbonization is used, larger openings are required at both ends of the carbonization furnace, and the subsequent oxygen diffuses into the furnace along with the material transport, causing oxidation of the materials in the furnace, and ultimately affects the mesophase pitch base. Properties of Carbon Fiber

Method used

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  • Gas sealing device for continuous carbonization furnace

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] Such as figure 1 As shown, a gas seal structure of a continuous carbonization furnace, including a front inlet pipe 1, a middle inlet pipe 2, a rear inlet pipe 3, a gas seal chamber 4, a gas distribution plate 5, a furnace port 9, and a material outlet 6 , insulation interlayer 7 and air-tight partition 8. A gas sealing device for a continuous carbonization furnace. The gas sealing device is divided into two parts, which are symmetrical up and down. The middle of the two parts is the material channel from the furnace port 9 to the material outlet 6, and the upper end from the furnace port 9 to the material outlet 6 is arranged in sequence. The front air intake pipe 1, the middle air intake pipe 2 and the rear air intake pipe 3 have the front air outlet pipe, the middle air outlet pipe and the rear air outlet pipe in turn at the lower end. The front air inlet pipe 1 is equipped with a branch pipe, which is located in the insulation interlayer 7. The insulation interlaye...

Embodiment 2

[0016] A gas seal structure of a continuous carbonization furnace, comprising a front intake pipe 1, a middle intake pipe 2, a rear intake pipe 3, a gas seal chamber 4, a gas distribution plate 5, a furnace port 9, a material outlet 6, and an insulating interlayer 7 and air-tight partition 8. It is characterized in that: the whole air seal is an open through type, the furnace port 9 is connected with the inside of the carbonization furnace, and the material outlet 6 is connected with the outside; the opening can be 10cm. The front inlet pipe controls the position and size of the air curtain through the size, arrangement and angle of the air holes. The diameter of the air holes is 3mm, the interval between adjacent air holes is 3mm, and the angle between the direction of the air holes and the vertical direction is 30°; The branch pipe of the inlet pipe is accompanied by auxiliary heating in the insulation interlayer, and the heating temperature is 600ºC. The central air pipe f...

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Abstract

The invention discloses a gas sealing device. The gas sealing device is suitable for gas sealing at the two ends of a continuous large-diameter carbonization furnace. The device comprises a front air inlet pipe, a middle air inlet pipe, a rear air inlet pipe, a gas seal chamber, a gas distribution disc, a furnace inner port, a material outlet, a heat insulation interlayer and a gas seal partition plate. The whole gas seal is in opening through type, the furnace inner port is connected with the inner portion of the carbonization furnace, and the material outlet is connected with the outside; a front inlet pipe controls the position and size of an air curtain through the size, arrangement and angle of an air hole, a branch pipe of the front inlet pipe is accompanied by auxiliary heating in the heat insulation interlayer to avoid the generation of an eddy; a middle gas pipe introduce inert gas into the inner portion of the gas seal chamber, and after the inert gas is distributed through the gas distribution disc, the multistage gas seal partition plate is formed into a multistage gas resistance layer for inhibiting oxygen diffusion; the rear air inlet pipe at the material outlet enhances the directional flow of the internal airflow from the inside to the outside, and inhibits the upward spread of the air. The opening degree of a furnace mouth can reach 10-30 centimeters, and the oxygen content can be reduced to less than or equal to 100 ppm.

Description

technical field [0001] The invention belongs to the field of carbonization treatment equipment for carbon fiber continuous filaments, in particular to an air-sealed structure of a continuous carbonization furnace, which is used for the carbonization treatment of mesophase pitch fiber pre-oxidized filaments in the key process in the preparation of pitch-based carbon fiber continuous filaments . Background technique [0002] The mesophase pitch fiber pre-oxidized yarn refers to the pre-oxidized pitch yarn obtained by the mesophase pitch fiber in an oxidizing atmosphere for non-melting treatment to improve thermal stability. In the subsequent carbonization process, the pre-oxidized filament can better maintain the shape of the fiber, and become a mesophase pitch-based carbon fiber with higher strength and modulus through the removal of non-carbon elements and the growth of crystals. On the one hand, since the strength of pre-oxidized filaments is only 10-50MPa, it is impossibl...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F9/32
CPCD01F9/322
Inventor 刘金水黄东叶崇吴邦廖超前齐绍忠
Owner 湖南纪璟新材料有限公司
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