A kind of manufacturing method of modified sepiolite fiber reinforced rubber asphalt
A sepiolite fiber and reinforced rubber technology, which is applied to building structures, building components, building insulation materials, etc., can solve the problems of high processing temperature, unsatisfactory construction workability, and low stability
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Embodiment 1
[0028] A method for manufacturing modified sepiolite fiber reinforced rubber asphalt, the specific steps comprising:
[0029] Step 1) Completely immerse the sepiolite fiber in a solution containing cyclodextrin and sodium hydroxide at 50°C for 12 minutes, remove and dry to obtain pretreated sepiolite fiber, the content of sodium hydroxide in the solution is 5 wt%, the content of cyclodextrin is 3 wt%,
[0030] Step 2) Put the pretreated sepiolite fiber into polyethylene glycol and cetyltrimethylammonium chloride aqueous solution, heat to 40°C and keep it warm for 12 minutes, while stirring magnetically, add titanate coupling after keeping warm agent, heated at 55°C for 30 minutes, filtered out the sepiolite fibers and dried in a blast drying oven at 45°C for 7 hours to obtain modified sepiolite fibers; the concentration of polyethylene glycol in the aqueous solution was 16g / L, Cetyltrimethylammonium chloride concentration is 7g / L,
[0031] Step 3) Mix 100 parts by mass of st...
Embodiment 2
[0034] A method for manufacturing modified sepiolite fiber reinforced rubber asphalt, the specific steps comprising:
[0035] Step 1) Completely immerse the sepiolite fiber in a solution containing cyclodextrin and sodium hydroxide at 55°C for 15 minutes, remove and dry to obtain pretreated sepiolite fiber, the content of sodium hydroxide in the solution is 6 wt%, the content of cyclodextrin is 4 wt%,
[0036] Step 2) Put the pretreated sepiolite fiber into polyethylene glycol and cetyltrimethylammonium chloride aqueous solution, heat to 45°C and keep it warm for 15 minutes, while stirring magnetically, add titanate coupling after keeping warm agent, heated at 55°C for 24 minutes, filtered out the sepiolite fibers and dried in a blast drying oven at 50°C for 6 hours to obtain modified sepiolite fibers; the concentration of polyethylene glycol in the aqueous solution was 18g / L, The concentration of cetyltrimethylammonium chloride is 8 g / L,
[0037] Step 3) Mix 100 parts by ma...
Embodiment 3
[0040] A method for manufacturing modified sepiolite fiber reinforced rubber asphalt, the specific steps comprising:
[0041] Step 1) Completely immerse the sepiolite fiber in a solution containing cyclodextrin and sodium hydroxide at 60°C for 13 minutes, remove and dry to obtain pretreated sepiolite fiber, the content of sodium hydroxide in the solution is 8 wt%, the content of cyclodextrin is 2 wt%,
[0042] Step 2) Put the pretreated sepiolite fiber into the aqueous solution of polyethylene glycol and cetyltrimethylammonium chloride, heat to 40°C and keep it for 14 minutes, while stirring magnetically, add titanate coupling after keeping it warm agent, heated at 50°C for 28 minutes, filtered out the sepiolite fibers and dried in a blast drying oven for 9 hours at 42°C to obtain modified sepiolite fibers; the concentration of polyethylene glycol in the aqueous solution was 17g / L, Cetyltrimethylammonium chloride concentration is 5 g / L,
[0043] Step 3) Mix 100 parts by mass...
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