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Preparation method of cynanchum wallichii wight root wall-breaking decoction pieces having efficacy of nourishing kidney, strengthening waist and strengthening bones and muscles, and cynanchum wallichii wight root wall-breaking decoction pieces prepared by preparation method

A technology of invigorating the kidney, strengthening the waist, and breaking the wall of decoction pieces, which is applied in the direction of medical preparations containing active ingredients, pharmaceutical formulas, block transportation, etc., can solve the problems of no industry norms and not widely used, and achieve the benefit of modern large-scale industrialization Development, stable quality, and good product composition consistency

Inactive Publication Date: 2019-06-07
JIANGXI GROUNDIONG PHARM CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the broken-wall decoction piece technology is not widely used in domestic decoction piece production enterprises, and no real industry norms have been formed.
Therefore, research and development of a preparation method of broken Chinese medicine decoction pieces, give full play to the advantages of using the whole ingredients of Chinese medicine broken wall decoction pieces, retain all the medicinal ingredients of traditional Chinese medicine by breaking the wall, which is more conducive to the absorption of medicinal ingredients by users , in order to alleviate the problem that the existing traditional Chinese medicine granules can only extract part of the medicinal ingredients after adding water to concentrate, it becomes very necessary and urgent
However, there is no report about the broken-walled decoction pieces of Duanjieshen and its preparation process at present.

Method used

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  • Preparation method of cynanchum wallichii wight root wall-breaking decoction pieces having efficacy of nourishing kidney, strengthening waist and strengthening bones and muscles, and cynanchum wallichii wight root wall-breaking decoction pieces prepared by preparation method
  • Preparation method of cynanchum wallichii wight root wall-breaking decoction pieces having efficacy of nourishing kidney, strengthening waist and strengthening bones and muscles, and cynanchum wallichii wight root wall-breaking decoction pieces prepared by preparation method

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Effect test

preparation example Construction

[0018] The preparation method of broken section ginseng broken wall decoction pieces of the present invention comprises the following steps:

[0019] (1) Take the dried ginseng medicinal material, pre-crushed to a particle size of 10-100 mesh, and then soak it with the first ethanol aqueous solution, wherein the concentration of the first ethanol aqueous solution is 30-60% by weight, and the soaking The conditions include: the temperature is 50-80°C, and the time is 1-3 hours;

[0020] (2) filtering, and freeze-drying the obtained filter cake, wherein the freeze-drying conditions include: the temperature is -10°C to -50°C, and the vacuum degree is 5-50Pa;

[0021] (3) placing the cooled ginseng granules at a temperature of -10°C to 0°C for 1-3 hours;

[0022] (4) placing the ginseng granules obtained in step (3) under vacuum conditions for microwave treatment;

[0023] (5) Superfinely pulverize the ginseng granules obtained in step (4);

[0024] (6) Mix the ultrafine powder...

Embodiment 1

[0039] (1) Take 2.0kg of sectioned ginseng medicinal material, pre-crushed to a particle size of 50 mesh particles, then add 45% by weight ethanol solution of 4 times the volume of sectioned ginseng particles, soak for 2 hours at 50°C, and use 200 mesh stainless steel wire Filter through a mesh, and freeze-dry the obtained filter cake at -20°C under a vacuum of 30 Pa. After the dried ginseng particles were dried, they were placed at -5°C for 2 hours.

[0040] (2) Put the ginseng granules obtained in step (1) under vacuum conditions for microwave treatment. The microwave treatment conditions are as follows: the temperature is 25°C, the time is 30min, the microwave power is 15kW, and the vacuum degree is 15Pa.

[0041] (3) Using a CW5-100QA broken wall ultrafine pulverizer to ultrafinely pulverize the ginseng granules obtained in step (2) to obtain ultrafine powder with a particle size of 5-30 microns.

[0042] (4) Mix the ultrafine powder with the ethanol aqueous solution with...

Embodiment 2

[0044] (1) Take 2.0 kg of sectioned ginseng medicinal material, pre-crushed to a particle size of 80 mesh particles, then add 60% by weight ethanol solution of 3 times the volume of sectioned ginseng particles, soak for 3 hours at 40 ° C, and use 200 mesh stainless steel wire The obtained filter cake was lyophilized at -30° C. under a vacuum of 20 Pa. After the dried ginseng particles were dried, they were placed at -8°C for 1 hour.

[0045] (2) Put the ginseng granules obtained in step (1) under vacuum conditions for microwave treatment. The microwave treatment conditions are as follows: the temperature is 20°C, the time is 40min, the microwave power is 10kW, and the vacuum degree is 10Pa.

[0046] (3) Using a CW5-100QA broken wall ultrafine pulverizer to ultrafinely pulverize the ginseng granules obtained in step (2) to obtain ultrafine powder with a particle size of 5-30 microns.

[0047] (4) Mix the ultrafine powder with the ethanol aqueous solution with a concentration o...

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Abstract

The invention relates to the technical field of traditional Chinese medicine wall-breaking decoction pieces, and discloses a preparation method of cynanchum wallichii wight root wall-breaking decoction pieces having efficacy of nourishing the kidney, strengthening the waist and strengthening bones and muscles, and the cynanchum wallichii wight root wall-breaking decoction pieces prepared by the preparation method The method comprises the following steps of (1) taking dry cynanchum wallichii wight root medicinal materials, performing pre-crushing to obtain granules of which the particle size is10-100 meshes, and performing soaking in first ethanol water; (2) performing filtration, and performing freeze drying on obtained filter cakes; (3) performing placing on the cynanchum wallichii wightroot granules after cooling treatment at the temperature of minus 10-0 DEG C for 1-3 hours; (4) performing microwave treatment on obtained cynanchum wallichii wight root granules obtained in the step(3) under the vacuum condition; (5) performing superfine crushing on the cynanchum wallichii wight root granules obtained in the step (4); and (6) mixing superfine fine powder obtained in the step (5) with second ethanol water, and then performing granulation and drying. Through the adoption of the method disclosed by the invention, the cynanchum wallichii wight root wall-breaking decoction pieces higher in wall-breaking rate can be prepared.

Description

technical field [0001] The invention relates to the technical field of broken-wall decoction pieces of traditional Chinese medicine, in particular to a method for preparing broken-section ginseng broken-wall decoction pieces with the functions of tonifying the kidney, strengthening the waist and strengthening bones and bones, and the broken-wall decoction pieces of Duanjie ginseng prepared therefrom. Background technique [0002] Broken-wall decoction pieces of traditional Chinese medicine is a traditional Chinese medicine decoction piece processed in powder form by using modern ultrafine pulverization technology. Broken wall decoction pieces of traditional Chinese medicine are all ingredients used as medicine, and the medicinal material basis remains unchanged, which is in line with the connotation of Chinese medicine decoction pieces. It can be directly brewed and taken together with the dregs of the medicine. However, the broken-wall decoction pieces technology is not wi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K9/16A61K36/27A61P1/14
Inventor 廖年生邹明明眭荣春罗云
Owner JIANGXI GROUNDIONG PHARM CO LTD
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