Graphene tightly coated SiO negative electrode material and preparation method thereof
A graphene-coated, negative-electrode material technology, applied to battery electrodes, electrical components, electrochemical generators, etc., can solve the problems of low theoretical capacity and poor cycle performance of silicon-based raw materials for battery negative electrodes, and achieve low cost and increased combination Strength, the effect of simple preparation process
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Embodiment 1
[0025] A kind of preparation method that can realize graphene tightly wrapping SiO negative electrode material, comprises the following steps:
[0026] 1) Preparation of surface-modified graphene oxide solution: use natural flake graphite as raw material, first prepare graphite oxide by modified Hummers method, centrifuge at 1000-15000rpm for 2min and wash with water to obtain graphene oxide slurry, according to the volume ratio Disperse the graphene oxide slurry in water with a ratio of 1:12 and ultrasonically for 3 minutes at 80W power, centrifuge at 1000-12000rpm for 2 minutes to remove unexfoliated graphite to obtain a graphene oxide solution, and add surface active material to the graphene oxide solution. agent, and disperse uniformly by ultrasonication for 3 minutes at a power of 80W to obtain a surface-modified graphene oxide solution;
[0027] 2) Preparation of SiO dispersion: SiO powder was added into an organic solvent, and stirred at 1000 rpm for 3 min to obtain a u...
Embodiment 2
[0033] The order number of natural flake graphite is 500 orders, and other processes are with embodiment 1.
[0034] The prepared graphene-coated SiO composite material and the SiO material without graphene coating were made into electrode sheets, and then assembled into button cells for electrochemical performance testing. Compared with SiO materials without graphene coating, under the same test conditions, the capacity increased by 21%, and the cycle performance increased by 30%.
Embodiment 3
[0036] The concentration of the graphene oxide solution was 5 mg / mL, and other processes were the same as in Example 1.
[0037] The prepared graphene-coated SiO composite material and the SiO material without graphene coating were made into electrode sheets, and then assembled into button cells for electrochemical performance testing. Compared with SiO materials without graphene coating, under the same test conditions, the capacity increased by 26%, and the cycle performance improved by 38%.
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