Method for preparing waterborne silicate zinc-enriched antirust and antiseptic paint from surface-activated and grafted glass flakes
A glass flake and surface activation technology, applied in anti-corrosion coatings, coatings, etc., can solve problems such as poor compatibility and affect the anti-corrosion performance of coatings, and achieve the effects of good compatibility, improved compatibility, and improved performance.
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0021] A method for preparing water-based silicate zinc-rich anti-rust and anti-corrosion paint with surface-activated grafted glass flakes is characterized in that it comprises the following steps:
[0022] (1) Preparation of surface-activated grafted glass flakes:
[0023] Add xylene to 16 parts of glass flakes at a ratio of 1:15, stir and disperse at high speed for 20 minutes, then add KH560 hydrolyzate dropwise at 60-65°C under nitrogen protection, raise the temperature to 80-85°C for 2 hours, then raise the temperature to 105-115°C React at ℃ for 50 minutes, wash with xylene for 3 times, wash with tetrahydrofuran for 2 times, Soxhlet purification for 10 hours, then vacuum dry at 110-113℃ to obtain glass flakes with surface-activated grafted KH560;
[0024] (2) Modification of mica iron oxide filler:
[0025] Add anhydrous toluene to 5 parts of micaceous iron oxide at 1:20, stir for 30 minutes and then ultrasonically treat for 20 minutes. Under nitrogen protection, add 3 ...
Embodiment 2
[0031] A method for preparing water-based silicate zinc-rich anti-rust and anti-corrosion paint with surface-activated grafted glass flakes is characterized in that it comprises the following steps:
[0032] (1) Preparation of surface-activated grafted glass flakes:
[0033] Add xylene to 20 parts of glass flakes at a ratio of 1:15, stir and disperse at high speed for 30 minutes, then add KH560 hydrolyzate dropwise at 60-65°C under nitrogen protection, heat up to 80-85°C for 3 hours, then raise the temperature to 105-115°C Reaction at ℃ for 70 minutes, washing with xylene 4 times and tetrahydrofuran 3 times, after Soxhlet purification for 12 hours, vacuum drying at 110-113 ℃ to obtain glass flakes with surface-activated grafted KH560;
[0034] (2) Modification of mica iron oxide filler:
[0035] Add anhydrous toluene to 10 parts of micaceous iron oxide at 1:20, stir for 40 minutes and then ultrasonically treat for 30 minutes. Under nitrogen protection, add 6 parts of toluene ...
PUM
Property | Measurement | Unit |
---|---|---|
thermal resistance | aaaaa | aaaaa |
hardness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com