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Paper file mould-proof bacteriostatic agent and preparation method thereof

A technology of anti-mildew, antibacterial, and paper archives, applied in the fields of botanical equipment and methods, fungicides, biocides, etc. Bacterial performance, improving the effect of anti-mildew and bacteriostatic time

Active Publication Date: 2019-02-22
QINGDAO UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, in addition to strict disinfection and dust removal before storage, paper files must also be treated with anti-mold and insect-proof drugs during storage to prevent mold and moths. Commonly used anti-mold and insect-proof drugs include camphor balls, sanitary balls, musk and Some chemical fumigants, etc., although camphor balls and hygienic balls have certain effects, most of their active ingredients contain p-dichlorobenzene, which can irritate the eyes, skin, mucous membranes and upper respiratory tract, and can be absorbed by the human body. Methemoglobin is formed to cause cyanosis. Chemical fumigants such as methyl bromide and ethylene oxide are toxic to the human body and are flammable and explosive.

Method used

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  • Paper file mould-proof bacteriostatic agent and preparation method thereof
  • Paper file mould-proof bacteriostatic agent and preparation method thereof
  • Paper file mould-proof bacteriostatic agent and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] An anti-fungal and bacteriostatic agent for paper archives, which is prepared from the following raw materials in parts by weight: 50 parts of porous carbon material, 3 parts of sodium citrate, 1 part of anchovy powder, 2 parts of asarum powder, and 3 parts of pepper powder , 1 part of Radix japonica oil, 2 parts of chitosan, 1 part of gelatin.

[0038] The preparation method of the described paper archives antifungal and bacteriostatic agent comprises the following steps:

[0039] (1) The porous carbon material was refluxed in concentrated nitric acid at 80° C. for 2 hours, acidified, and then washed to neutrality for later use;

[0040] (2) Dissolve sodium citrate in acetic acid solution, add anchovy powder, Chinese prickly ash powder, asarum powder, Radix japonica oil, chitosan and porous carbon material, and perform high pressure homogenization after ultrasonic dispersion for 10 min. The pressure is 30MPa, and the homogenization time is 10min;

[0041] (3) adding ...

Embodiment 2

[0051] An anti-fungal and bacteriostatic agent for paper archives, which is made from the following raw materials in parts by weight: 88 parts of porous carbon materials, 5 parts of sodium citrate, 4 parts of anchovy powder, 4 parts of asarum powder, and 6 parts of pepper powder , 2 parts of Radix japonica oil, 6 parts of chitosan, and 3 parts of gelatin.

[0052] The preparation method of the described paper archives antifungal and bacteriostatic agent comprises the following steps:

[0053] (1) The porous carbon material was refluxed in concentrated nitric acid at 80°C for 3 hours, acidified, and then washed to neutrality for later use;

[0054] (2) Dissolve sodium citrate in acetic acid solution, add anchovy powder, Chinese prickly ash powder, asarum powder, Radix japonica oil, chitosan and porous carbon material, and perform high pressure homogenization after ultrasonic dispersion for 10 min. The pressure is 75MPa, and the homogenization time is 5min;

[0055] (3) adding...

Embodiment 3

[0065] An anti-fungal and bacteriostatic agent for paper archives, which is made from the following raw materials in parts by weight: 70 parts of porous carbon material, 4 parts of sodium citrate, 2 parts of anchovy powder, 3 parts of asarum powder, and 4 parts of pepper powder , 1.5 parts of arborvitae oil, 5 parts of chitosan, and 2 parts of gelatin.

[0066] Wherein, the preparation method of the porous carbon material is:

[0067] (1) prepare the sodium hydroxide solution that mass fraction is 7%, put the loofah into the sodium hydroxide solution and soak it for 5-10min, wherein, the mass ratio of the loofah to the sodium hydroxide solution is 1:15, then heated to Stir at 50°C for 30min, wash, dry and pulverize;

[0068] (2) take by weighing triethanolamine dodecyl sulfate, butyl acrylate and be dispersed in distilled water, then add the loofah powder obtained in step (1), the quality of triethanolamine dodecyl sulfate, butyl acrylate, loofah The ratio is 1: 1.5: 40, sti...

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PUM

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Abstract

The invention belongs to the technical field of file protection, and discloses a paper file mould-proof bacteriostatic agent and a preparation method thereof. The paper file mould-proof bacteriostaticagent is prepared from the following raw materials in parts by weight: 50-88 parts of a porous carbon material, 3-5 parts of sodium citrate, 1-4 parts of herba pteridis multifidae powder, 2-4 parts of herba asari powder, 3-6 parts of pricklyash peel powder, 1-2 parts of litsea cubeba oil, 2-6 parts of chitosan and 1-3 parts of gelatin. The paper file mould-proof bacteriostatic agent of a microsphere structure is prepared through the steps of ultrasoundphonic, high- pressure homogenization, gelling, liquid nitrogen freezing and the like of the porous carbon material, the sodium citrate, the herba pteridis multifidae powder, the herba asari powder, the pricklyash peel powder, the litsea cubeba oil, the chitosan and the gelatin, the synergistic effect is achieved through raw material compounding, thus the mould-proof bacteriostatic time can be effectively prolonged, the paper file mould-proof bacteriostatic agent is good in mould-proof bacteriostatic effect, has no toxic and side effectson a human body, has no pollution to the environment and no impact on paper files, is not prone to burning, and can be used safely.

Description

technical field [0001] The invention belongs to the technical field of archives protection, and relates to a paper archives anti-mildew and bacteriostatic agent and a preparation method thereof. Background technique [0002] With the continuous enhancement of people's awareness of archives, the use of archives has become more and more popular, but archives management has the problem of "focusing on collection and ignoring protection". At present, most archives are still kept in paper form. Mold erosion has always been one of the most important problems faced in the protection of paper archives, and it is also a key factor affecting the life of paper archives. [0003] At present, in addition to strict disinfection and dust removal before the paper files are put into storage, anti-mold and insect-proof drugs should be applied during the storage period to prevent mildew and moths. Commonly used anti-mold and insect-proof drugs include mothballs, sanitary balls, musk and Some...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N65/08A01N65/36A01N65/04A01N65/24A01N43/40A01N59/00A01N37/36A01P1/00A01P3/00
CPCA01N37/36A01N43/40A01N59/00A01N65/00A01N65/04A01N65/08A01N65/24A01N65/36
Inventor 杨洪云葛兆富张楠于健苟煜林
Owner QINGDAO UNIV
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