Compound eluting agent and method for eluting heavy metals in soil by virtue of compound eluting agent
A compound eluent and eluent technology, applied in the restoration of contaminated soil, soil conditioning materials, chemical instruments and methods, etc., can solve the problems of secondary pollution, eluent pollution, etc., and achieve short time and environmental protection Friendly, rinse-enhancing effect
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Embodiment 1
[0026] Prepare eluent: dissolve oxalic acid and tea saponin in water, adjust the pH to 6 with sodium hydroxide, wherein the concentration of oxalic acid is 0.1 mol / L, and the mass concentration of tea saponin is 2%.
[0027] Rinse: Carry out experiments at room temperature, with the optimum water-to-soil ratio of 20:1, weigh 1g of 1# soil sample passed through a 100-mesh sieve into a 50ml centrifuge tube, add 20ml of the above-mentioned eluent into the centrifuge tube, at 25 Centrifuge at 150r / min for 2 hours at 150r / min, put the centrifuge tube into a centrifuge, centrifuge at 4000r / min for 15min, pass through a 0.45μm filter, put the filtrate into a 15ml centrifuge tube, and use inductive coupling The content of As and Cd was measured by plasma mass spectrometry (ICP-MS).
[0028] The results show that the removal rate of As in 1# soil sample by the eluent of this example is 90%, and the removal rate of Cd is 45%.
Embodiment 2
[0030] Prepare eluent: dissolve oxalic acid and tea saponin in water, adjust the pH to 6 with sodium hydroxide, wherein the concentration of oxalic acid is 0.1 mol / L, and the mass concentration of tea saponin is 2%.
[0031] Rinse: Carry out experiments at room temperature, with the optimum water-to-soil ratio of 20:1, weigh 1g of 1# soil sample passed through a 100-mesh sieve into a 50ml centrifuge tube, add 20ml of the above-mentioned eluent into the centrifuge tube, at 25 At ℃, shake at 150r / min for 0.5h. After shaking, put the centrifuge tube into the centrifuge, centrifuge at 4000r / min for 15min, pass through a 0.45μm filter membrane, and put the filtrate into a 15ml centrifuge tube. The content of As and Cd was measured by coupled plasma mass spectrometry (ICP-MS).
[0032] The results show that the removal rate of As in 1# soil sample by the eluent of this example is 75%, and the removal rate of Cd is 31%.
Embodiment 3
[0034] Prepare eluent: dissolve oxalic acid and tea saponin in water, adjust the pH to 6 with sodium hydroxide, wherein the concentration of oxalic acid is 0.1 mol / L, and the mass concentration of tea saponin is 2%.
[0035] Rinse: Carry out experiments at room temperature, with the optimum water-to-soil ratio of 20:1, weigh 1g of 1# soil sample passed through a 100-mesh sieve into a 50ml centrifuge tube, add 20ml of the above-mentioned eluent into the centrifuge tube, at 25 Centrifuge at 150r / min for 1 hour at 150r / min, put the centrifuge tube into a centrifuge, centrifuge at 4000r / min for 15min, pass through a 0.45μm filter, put the filtrate into a 15ml centrifuge tube, and use inductive coupling The content of As and Cd was measured by plasma mass spectrometry (ICP-MS).
[0036] The results show that the removal rate of As in the 1# soil sample by the eluent of this example is 79%, and the removal rate of Cd is 37%.
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