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A kind of regeneration method of waste gypsum model

A technology for waste gypsum and models, applied in the field of gypsum, can solve the problems of long mold casting time, low strength of gypsum powder, shortening the initial and final setting time of gypsum powder, etc., so as to improve the strength, prolong the initial setting time, and prolong the initial and final setting time. Effect

Active Publication Date: 2021-01-05
厦门佳浴智能卫浴有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Special attention should be paid to the fact that the waste gypsum model contains a certain amount of sodium sulfate and anhydrous calcium sulfate, which makes the strength of the regenerated gypsum powder low. Among them, sodium sulfate is easy to absorb water and expand, and the pressure generated by water absorption and expansion is easy to make the model cracked. The strength of the gypsum model made of recycled gypsum powder is reduced, and sodium sulfate will also shorten the initial and final setting time of the gypsum powder. The volume of the gypsum model for sanitary ceramics is usually large, and the pouring time is usually relatively long. If the initial setting time is too short, Then the workers do not have time to operate, making it difficult to complete the grouting

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  • A kind of regeneration method of waste gypsum model

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Embodiment 1

[0045]This embodiment provides a regeneration method for waste gypsum models. The collected waste gypsum models are broken open and sorted. After being crushed, pass through a 60-mesh sieve to obtain coarse waste gypsum particles and transfer them to a stirring tank, add water equivalent to 4 times the weight of waste gypsum coarse particles, and stir at 40°C for 1.5 hours. Centrifuge while hot, discard the filtrate, add 4 times the mass of 10% hydrogen peroxide to the filter residue, stir for 1.5 hours, discard the filtrate after filtration, transfer the filter residue to a sedimentation tank, add water equivalent to 3 times the weight of the filter residue, adjust the pH to 5.0, Stand still for 12 hours, remove the supernatant, remove the lower layer of sediment and place it in an autoclave, and autoclave at a temperature of 125°C and a pressure of 0.3 MPa for 2 hours. After the autoclave is completed, open the pressure relief valve to release the pressure. Dry it at 135°C f...

Embodiment 2

[0047] This embodiment provides a regeneration method for waste gypsum models. The collected waste gypsum models are broken open and sorted. After being crushed, pass through an 80-mesh sieve to obtain coarse particles of waste gypsum and transfer them to a stirring tank, add water equivalent to 5 times the weight of coarse particles of waste gypsum, and stir at 55°C for 1.0 hour. Centrifuge while hot, discard the filtrate, add 5 times the mass of 10% hydrogen peroxide to the filter residue, stir for 2 hours, discard the filtrate after filtration, transfer the filter residue to a sedimentation tank, add water equivalent to 2 times the weight of the filter residue, and adjust the pH to 4. Stand still for 6 hours, remove the supernatant liquid, take the lower layer of sediment and place it in an autoclave, and autoclave it at a temperature of 120°C and a pressure of 0.2MPa for 3.5 hours. After the autoclave is over, open the pressure relief valve to release the pressure. Dry it ...

Embodiment 3

[0049] This embodiment provides a regeneration method for waste gypsum models. The collected waste gypsum models are broken open and sorted. After being crushed, pass through a 60-mesh sieve to obtain coarse waste gypsum particles and transfer them to a stirring tank, add water equivalent to 3 times the weight of waste gypsum coarse particles, and stir for 2 hours at 35°C. Centrifuge while hot, discard the filtrate, add 5% hydrogen peroxide with 4 times the mass to the filter residue, stir for 1 hour, discard the filtrate after filtering, transfer the filter residue to a sedimentation tank, add water equivalent to 4 times the weight of the filter residue, and adjust the pH to 6. Stand still for 18 hours, remove the supernatant, remove the lower layer of sediment and place it in an autoclave, and autoclave at a temperature of 130°C and a pressure of 0.4MPa for 1.5 hours. After the autoclave is over, open the pressure relief valve to release the pressure. Bake at 150°C for 4 hou...

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Abstract

The invention relates to a method for regenerating a waste gypsum model, and belongs to the field of gypsum. The method comprises the following steps: (1) crushing: crushing the waste gypsum model, and sieving with a sieve of 60-80 mesh to obtain coarse waste gypsum particles; (2) primary purification: adding water into the waste gypsum granules, stirring, and filtering to obtain filter residue A;(3) secondary purification: adding hydrogen peroxide into the filter residue A, stirring, and filtering to obtain filter residue B; (4) tertiary purification: adding water into the filter residue B,adjusting a pH value to 4-6, standing still, and removing supernatant to obtain underlying sediment; (5) autoclaving and drying: autoclaving the underlying sediment, and drying to obtain a drying material; and (6) grinding: mixing the drying material with polyacrylamide for grinding. By adopting the method provided by the invention, impurities in the waste gypsum model can be effectively removed,and the gypsum powder obtained with the regeneration method has relatively high strength when used for preparing the gypsum model.

Description

technical field [0001] The invention relates to the field of gypsum, in particular to a method for regenerating a waste gypsum model. Background technique [0002] Sanitary ceramic products are important supplies in people's lives. One of the main molding methods for producing sanitary ceramics is slip casting, and most of the slip casting is done with mud in a plaster model. Plaster models are usually used dozens of times and can no longer be used, becoming discarded waste plaster models. The production of daily-use porcelain also has a large number of discarded waste plaster models. According to statistics, the waste gypsum models that are only used to make ceramic products in China are as high as several million tons every year. At present, the utilization of waste gypsum models is mainly used by cement enterprises as part of the raw materials, but the amount of use is limited. Therefore, the waste plaster models in many ceramic production areas have become garbage th...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B11/26
CPCC04B11/262
Inventor 李小满
Owner 厦门佳浴智能卫浴有限公司
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