Ferrotitanium alloy hydrogen storage material used for fuel cell car and preparing method
A technology of titanium-iron alloy and hydrogen storage material, which is applied in metal processing equipment, transportation and packaging, etc., can solve the problems of poor activation and stability of titanium-iron hydrogen storage alloy, poor resistance to gaseous impurity poisoning, difficult alloy surface activation, etc. Improved activation and stability, long service life and low cost
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Embodiment 1
[0030] a. Using tetraethyl orthosilicate as a solvent, slowly add a saturated aqueous solution containing iron trichloride and titanium tetrachloride dropwise, while adding a reducing agent, a pore-forming agent and a flocculant for stirring, and using citric acid to adjust the pH value to 4 , standing and aging after complete reaction to obtain a gel-like material;
[0031] b. Uniformly mixing the gel-like material prepared in step a with doped metal powder, performing low-temperature heat treatment under the mixed gas source of argon / hydrogen, and then performing subsequent molding to obtain a titanium-iron alloy hydrogen storage material.
[0032]In step a, the reducing agent is lithium aluminum hydride, the pore forming agent is sodium bicarbonate, and the flocculant is aluminum sulfate; in step b, the doped metal powder is manganese powder;
[0033] In step a, 56 parts by weight of ethyl orthosilicate, 18 parts by weight of iron salt, 18 parts by weight of titanium salt, ...
Embodiment 2
[0036] a. Using tetraethyl orthosilicate as a solvent, slowly add a saturated aqueous solution containing iron trichloride and titanium tetrachloride dropwise, while adding a reducing agent, a pore-forming agent and a flocculant for stirring, and using citric acid to adjust the pH value to 4 , standing and aging after complete reaction to obtain a gel-like material;
[0037] b. Uniformly mixing the gel-like material prepared in step a with doped metal powder, performing low-temperature heat treatment under the mixed gas source of argon / hydrogen, and then performing subsequent molding to obtain a titanium-iron alloy hydrogen storage material.
[0038] In step a, the reducing agent is stannous chloride, the pore forming agent is potassium bicarbonate, and the flocculant is aluminum chloride; in step b, the doped metal powder is magnesium powder;
[0039] In step a, 65 parts by weight of ethyl orthosilicate, 15 parts by weight of iron salt, 15 parts by weight of titanium salt, 3 ...
Embodiment 3
[0042] a. Using tetraethyl orthosilicate as a solvent, slowly add a saturated aqueous solution containing iron trichloride and titanium tetrachloride dropwise, while adding a reducing agent, a pore-forming agent and a flocculant for stirring, and using citric acid to adjust the pH value to 4 , standing and aging after complete reaction to obtain a gel-like material;
[0043] b. Uniformly mixing the gel-like material prepared in step a with doped metal powder, performing low-temperature heat treatment under the mixed gas source of argon / hydrogen, and then performing subsequent molding to obtain a titanium-iron alloy hydrogen storage material.
[0044] In step a, the reducing agent is potassium borohydride, the pore-forming agent is ammonium bicarbonate, and the flocculant is ferric sulfate; in step b, the doped metal powder is manganese powder;
[0045] In step a, 50 parts by weight of ethyl orthosilicate, 20 parts by weight of iron salt, 20 parts by weight of titanium salt, 5 ...
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