Platinum atom-loaded titanium dioxide photocatalytic material and preparation method thereof
A photocatalytic material, titanium dioxide technology, applied in the field of photocatalytic materials, can solve the problems of not being able to fully utilize solar energy, and achieve the effects of increasing the photoresponse range, enhancing active sites, and good photocatalytic hydrogen production effects
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0031] a. Add 0.3g of ascorbic acid into 100mL of deionized water, and keep stirring for 10 minutes to obtain a transparent solution;
[0032] b. Add 3.1mL titanium trichloride (commercially available titanium trichloride aqueous solution, mass fraction: 37%) to the transparent solution in step a to form a purple solution, then add 1mol / L sodium hydroxide solution until the pH value was 4.5, and continued to stir for 30 minutes to obtain a black titanium dioxide suspension;
[0033] c. Transfer the solution in step b to a 100mL hydrothermal reaction kettle, and react at a temperature of 180°C for 12 hours to obtain a nano-titanium dioxide mixed solution;
[0034] d. Wash the nano black titanium dioxide in step c through 50mL deionized water and 50mL ethanol to pH 7 respectively, and dry to obtain the nano titanium dioxide photocatalyst;
[0035] e. Weigh 0.2 g of the titanium dioxide powder obtained in step d, add it to 400 mL of deionized water, and obtain a uniform titanium...
Embodiment 2
[0040] a. Add 0.7g of ascorbic acid into 70mL of deionized water, and keep stirring for 10 minutes to obtain a transparent solution;
[0041] b. Add 3.1mL titanium trichloride (commercially available titanium trichloride aqueous solution, mass fraction: 37%) to the transparent solution in step a to form a purple solution, then add 1mol / L sodium hydroxide solution until the pH value was 4.5, and continued to stir for 30 minutes to obtain a black titanium dioxide suspension;
[0042] c. Transfer the solution in step b to a 100mL hydrothermal reaction kettle, and react at a temperature of 180°C for 12 hours to obtain a nano-titanium dioxide mixed solution;
[0043] d. Wash the nano black titanium dioxide in step c through 50mL deionized water and 50mL ethanol to pH 7 respectively, and dry to obtain the nano titanium dioxide photocatalyst;
[0044] e. Weigh 0.2 g of the titanium dioxide powder obtained in step d, add it to 200 mL of deionized water, and obtain a uniform titanium ...
Embodiment 3
[0049] a. Add 0.7g of ascorbic acid into 70mL of deionized water, and keep stirring for 10 minutes to obtain a transparent solution;
[0050] b. Add 3.1mL titanium trichloride (commercially available titanium trichloride aqueous solution, mass fraction is 37%) to the transparent solution of step a to form a purple solution, then add 10mol / L sodium hydroxide solution until the pH value was 4.5, and continued to stir for 30 minutes to obtain a black titanium dioxide suspension;
[0051] c. Transfer the solution in step b to a 100mL hydrothermal reaction kettle, and react at a temperature of 180°C for 12 hours to obtain a nano-titanium dioxide mixed solution;
[0052] d. Wash the nano black titanium dioxide in step c through 50mL deionized water and 50mL ethanol to pH 7 respectively, and dry to obtain the nano titanium dioxide photocatalyst;
[0053]e. Weigh 0.2 g of the titanium dioxide powder obtained in step d, add it to 200 mL of deionized water, and obtain a uniform titaniu...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com