Composite catalyst for degrading antibiotics by visible light
A technology of composite catalysts and antibiotics, applied in the field of environmental chemistry, can solve the problem of difficult recovery of catalysts, and achieve the effects of good physical and chemical properties, improved catalytic efficiency, and excellent photocatalytic performance.
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Embodiment 1
[0013] Measure 20mL 0.1mol / L AgNO 3 Aqueous solution, 10mL 0.1mol / L Na 2 MoO 4 Add 0.02 g of polyethylene glycol to the aqueous solution, place the two solutions on both sides of the casing, let stand for 10 hours to react until the system fully reacts, take the precipitates on both sides of the casing, wash and dry to obtain graphene powder; Put 1 g of graphene powder and 0.5 g of the nano-silver deposited silver molybdate catalyst obtained by repeating the above steps several times into a beaker, use absolute ethanol as the medium, and ultrasonically disperse for 1 hour, then suction filter the dispersed system, and then Dried in oven, obtains graphene / silver molybdate nanocomposite catalyst; Graphene / silver molybdate nanocomposite catalyst is irradiated for 10 minutes under the ultraviolet light of 20W power, obtains graphene / nanometer silver deposition silver molybdate nanocomposite catalyst . Add 0.1 g of composite catalyst, use it to degrade 50 mL of tetracycline hydr...
Embodiment 2
[0015] Measure 20mL 0.1mol / L AgNO 3 Aqueous solution, 10mL 0.1mol / L Na 2 MoO 4 Add 0.02g of Triton x-100 to the aqueous solution, place the two solutions on both sides of the casing, let it stand for 10 hours to react until the system fully reacts, take the precipitates on both sides of the swim bladder, wash and dry to obtain graphene powder body; 1 g of graphene powder and 1 g of the nano-silver deposited silver molybdate catalyst obtained by repeating the above-mentioned steps are put into a beaker, and with absolute ethanol as the medium, after ultrasonic dispersion for 1 hour, the dispersed system is suction-filtered, Dry in oven again, obtain graphene / silver molybdate nanocomposite catalyst; Graphene / silver molybdate nanocomposite catalyst irradiates 10 minutes under the ultraviolet light of 20W power, obtains graphene / nanometer silver deposition silver molybdate nanocomposite catalyst. Add 0.1 g of composite catalyst, use it to degrade 50 mL of tetracycline hydrochlo...
Embodiment 3
[0017] Measure 20mL 0.1mol / L AgNO 3 Aqueous solution, 10mL 0.1mol / L Na 2 MoO 4 Add 0.02 g of polyethylene glycol to the aqueous solution, place the two solutions on both sides of the casing, let stand for 10 hours to react until the system fully reacts, take the precipitates on both sides of the casing, wash and dry to obtain graphene powder; Put 2 g of graphene powder and 0.5 g of the nano-silver deposited silver molybdate catalyst obtained by repeating the above steps several times into a beaker, use absolute ethanol as the medium, and ultrasonically disperse for 1 hour, then suction filter the dispersed system, and then Dried in an oven to obtain a graphene / silver molybdate nanocomposite catalyst; the graphene / silver molybdate nanocomposite catalyst was irradiated for 8 minutes under the ultraviolet light of 20W power to obtain a graphene / nanometer silver deposition silver molybdate nanocomposite catalyst . Add 0.1 g of composite catalyst, use it to degrade 50 mL of tetr...
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