A kind of noise reduction material, its preparation method and automobile engine cover
A noise reduction and cork technology, applied in the field of noise reduction materials and car hoods, can solve the problems of increasing the cost of vehicles, the inability to take into account the mechanical properties and light weight, etc., to ensure light weight, ensure sound absorption and sound insulation effect, and enhance mechanical properties. Effect
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[0025] The embodiment of the present invention discloses a method for preparing a noise reducing material, comprising the following steps:
[0026] Step S1: treating granular cork and fibrous cork with pectinase, and drying to obtain enzymolyzed cork material;
[0027] Step S2: Ultrasonic impregnation of the enzymolyzed cork material with a mixture of tetraethylorthosilicate and isocyanate to obtain an impregnated cork material;
[0028] Step S3: using a thermosetting resin to heat and press the impregnated cork material to obtain a noise reducing material.
[0029] The invention uses two types of cork with different shapes as base materials, and obtains the noise-reducing material through a series of treatments. The combined use of the cork materials with the two shapes can increase the contact points between the base materials, and the mechanical strength of the material can be improved after being glued by the thermosetting resin.
[0030] The following describes the prep...
Embodiment 1
[0054]The granular cork and the fibrous cork are treated with pectinase at 40° C. for 3 hours and then dried to control the water content of the enzymolyzed cork material to be 3% to 5%.
[0055] Ultrasonic impregnation of the enzymatically hydrolyzed cork material with a mixture of tetraethyl orthosilicate and isocyanate at a mass ratio of 1:1, the ultrasonic frequency of the ultrasonic impregnation is 45kHz, the time is preferably 4h, and the temperature is 35°C to obtain impregnated After the cork material;
[0056] Use epoxy resin to cure the impregnated cork material by hot pressing, the mass ratio of epoxy resin to impregnated cork material is 1:1, the hot pressing temperature is 140°C, and the hot pressing pressure is 10MPa to obtain the noise reduction material .
[0057] The lightweight data and mechanical properties of the prepared noise reduction material were tested. The experimental results showed that the noise reduction material prepared in this example had a b...
Embodiment 2
[0064] Use pectinase to treat granular cork with a particle size of 80-500 microns and fibrous cork with an aspect ratio of 50:1 at 40°C. After 5 hours of treatment, dry it to control the enzymolysis. The moisture content of the cork material is 3% to 5%.
[0065] Ultrasonic impregnation of the enzymatically hydrolyzed cork material with a mixture of tetraethyl orthosilicate and isocyanate at a mass ratio of 1:2, the ultrasonic frequency of the ultrasonic impregnation is 50kHz, the time is preferably 3h, and the temperature is 40°C to obtain impregnated After the cork material;
[0066] The impregnated cork material is cured by hot pressing with liquid phenolic resin, the mass ratio of liquid phenolic resin to the impregnated cork material is 2:1, the hot pressing temperature is 150°C, and the hot pressing pressure is 15MPa to obtain the noise reduction material .
[0067] The lightweight data and mechanical properties of the prepared noise-reducing material were tested, and...
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