Method for preparing copper metal nanopowder having uniform oxygen passivation layer by using thermal plasma, and apparatus for preparing same
A metal powder and powder technology, which is applied in the field of preparing copper metal nano-powder with a uniform oxygen passivation layer by using thermal plasma and its preparation equipment, can solve the problems of high purity limitation, difficulty and the like
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example 1
[0052] Copper powder having an average particle diameter of 12 μm and a purity of 96% was supplied into the plasma high temperature region by a raw material supplier at an injection rate of 0.5 kg / hr. Treatment with RF thermal plasma with 4MHz high-frequency power supply frequency, such as figure 1 As shown in , the raw material powder is melted due to thermal plasma. Under the condition that the amount of oxygen added is 1 slpm for 1 kg of copper or copper alloy powder injected per hour, oxygen passes through the oxygen reaction area to form a surface oxygen passivation layer. Afterwards, the oxygen that has passed through the reaction vessel to generate powder and the nano-copper metal powder that has been uniformly passivated by oxygen are collected by the collector. As a result, nano copper metal powder having an average particle diameter of 79 nm and an oxygen passivation layer having a thickness of 10 to 15 nm was prepared.
example 2
[0054] Nano copper metal powder having an average particle diameter of 98 nm and an oxygen passivation layer with a thickness of 8 to 10 nm was prepared in the same manner as Example 1 except that the injection rate of the copper powder was 0.9 kg / hr.
example 3
[0056] Nano copper metal powder having an average particle diameter of 120 nm and an oxygen passivation layer thickness of 5 to 8 nm was prepared in the same manner as Example 1 except that the injection rate of the copper powder was 1.2 kg / hr.
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