Oral liquid containing radix acanthopanacis senticosi and method for extracting eleutherosides from radix acanthopanacis senticosi
A technology of total glucosides and extraction methods of Acanthopanax senticosus, which is applied in the directions of pharmaceutical formulations, dispersion liquid delivery, medical preparations containing active ingredients, etc. , do not pay attention to sample pretreatment and other issues, to achieve the effect of good medicinal activity, simple and feasible operation, and short extraction time
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Embodiment 1
[0038] A method for extracting eleutherosides from Acanthopanax ginseng, the steps are as follows:
[0039] Step a, five ginseng raw material pretreatment:
[0040] a1: Select fresh raw materials of Wujiaginseng, clean them and dry them in a vacuum drying oven at 60-65°C for 10-15 hours, and crush the fully dried raw materials of Wujiaginseng into 50-100 meshes;
[0041] a2: Add petroleum ether to the Wujiashen powder obtained in step a1, the mass volume ratio of the Wujiashen powder to petroleum ether is 1g:5-10mL, reflux and extract for 2-3h, filter and remove the filtrate, and put the filter residue into Dry in a vacuum oven at 50°C for 30 minutes to volatilize the solvent, and obtain the defatted Wujiaginseng powder from which the fat-soluble impurities in the chlorophyll have been removed;
[0042] Step b, high-pressure extraction of total eleutherosides in defatted Radix Acanthopanax ginseng powder:
[0043] b1: Add 40% ethanol solution to the defatted Wujiashen powder...
Embodiment 2
[0053] A method for extracting eleutherosides from Acanthopanax ginseng, the steps are as follows:
[0054] Step a, five ginseng raw material pretreatment:
[0055] a1: Select fresh roots of Radix Radix Radix Acanthus Radix, after cleaning, dry them in a vacuum drying oven at 60°C for 10 hours, and crush the raw materials of Radix Radix Radix Radix Radix Radix L. after fully drying to 50 meshes;
[0056] a2: Add petroleum ether to the Wujiashen powder obtained in step a1, the mass volume ratio of the Wujiashen powder to petroleum ether is 1g:5mL, reflux and extract for 2 hours, filter and remove the filtrate, and put the filter residue at 50°C for vacuum drying Dry in the box for 30 minutes to volatilize the solvent, and obtain the defatted Wujiaginseng powder from which the fat-soluble impurities in the chlorophyll have been removed;
[0057] Step b, high-pressure extraction of total eleutherosides in defatted Radix Acanthopanax ginseng powder:
[0058] b1: Add 40% ethanol ...
Embodiment 3
[0071] A method for extracting eleutherosides from Acanthopanax ginseng, the steps are as follows:
[0072] Step a, five ginseng raw material pretreatment:
[0073] a1: Select fresh stems of Radix Radix Radix, clean and dry them in a vacuum drying oven at 62°C for 12 hours, and crush the raw materials of Radix Radix Radix to 80 meshes after fully drying;
[0074] a2: Add petroleum ether to the Wujiashen powder obtained in step a1, the mass volume ratio of the Wujiashen powder to petroleum ether is 1g:6mL, filter and remove the filtrate after reflux extraction for 3 hours, and put the filter residue at 50°C for vacuum drying Dry in the box for 30 minutes to volatilize the solvent, and obtain the defatted Wujiaginseng powder from which the fat-soluble impurities in the chlorophyll have been removed;
[0075] Step b, high-pressure extraction of total eleutherosides in defatted Radix Acanthopanax ginseng powder:
[0076] b1: Add 40% ethanol solution to the degreased Acanthopanax...
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