Method for recycling paraffin from polytetrafluoroethylene resin kettle-cleaning material
A polytetrafluoroethylene resin and polytetrafluoroethylene technology, which is applied in the field of recycling paraffin, can solve the problems such as no public reports of polytetrafluoroethylene resin tank cleaning materials and paraffin separation and purification methods, and achieve the improvement of resource utilization value, Realize the effect of productization and high product purity
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Embodiment 1
[0045] The present embodiment provides a method for reclaiming paraffin wax from polytetrafluoroethylene resin cleaning material, the specific steps of the method are as follows: in a reaction kettle with a volume of 500L, add 200kg polytetrafluoroethylene resin cleaning material (wherein , by weight, polytetrafluoroethylene resin 35%, water 5% and paraffin 60%) and 100kg deionized water, control temperature 60-65 ℃, time 1h, stir 0.5h after melting, finish washing with water. Stand for stratification for 1 hour, start the vacuum pump, suck the upper layer of paraffin liquid into the dryer, start the stirring and vacuum system of the dryer, turn on the steam heating device, and implement the drying and dehydration operation. Control temperature 80~100℃, drying time 0.5h, vacuum degree -0.08MPa~-0.09MPa. After drying, start the precision filter device, pump the paraffin to the filter under pressure, and perform the filter operation, the filter pressure is 1.5kgf / cm 2 . The fi...
Embodiment 2
[0053] The present embodiment provides a method for reclaiming paraffin wax from polytetrafluoroethylene resin cleaning material, the specific steps of the method are as follows: in a reaction kettle with a volume of 500L, add 200kg polytetrafluoroethylene resin cleaning material (wherein , by weight, polytetrafluoroethylene resin 35%, water 5% and paraffin 60%) and 150kg deionized water, control temperature 70-80 ℃, time 1h, stir 1h after melting, finish washing. Stand for stratification for 1 hour, start the vacuum pump, suck the upper layer of paraffin liquid into the dryer, start the stirring and vacuum system of the dryer, turn on the steam heating device, and implement the drying and dehydration operation. Control temperature 80~100℃, drying time 0.5h, vacuum degree -0.08MPa~-0.09MPa. After drying, start the precision filter device, pump the paraffin to the filter under pressure, and carry out the filter operation, the filter pressure is 1.0kgf / cm 2 . The filtrate flow...
Embodiment 3
[0061] The present embodiment provides a method for reclaiming paraffin wax from polytetrafluoroethylene resin cleaning material, the specific steps of the method are as follows: in a reaction kettle with a volume of 500L, add 200kg polytetrafluoroethylene resin cleaning material (wherein , by weight, polytetrafluoroethylene resin 35%, water 5% and paraffin 60%) and 200kg deionized water, control temperature 70-80 ℃, time 1.5h, stir 1h after melting, finish washing with water. Stand for stratification for 2 hours, start the vacuum pump, suck the paraffin liquid in the upper layer into the desiccator, start the stirring and vacuum system of the desiccator, turn on the steam heating device, and implement the drying and dehydration operation. Control temperature 80~100℃, drying time 0.5h, vacuum degree -0.08MPa~-0.09MPa. After drying, start the precision filter device, pump the paraffin to the filter under pressure, and carry out the filter operation, the filter pressure is 3kgf / ...
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