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A kind of decolorization method of Sapindus saponin

A technology of sapindus saponin and decolorizing agent, which is applied in the field of biochemical research, can solve the problems of high loss rate of target product, poor decolorization effect, and pollute the environment, and achieves better decolorization effect, low production cost and less dosage. Effect

Active Publication Date: 2020-11-10
JIANGXI NORMAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] In order to overcome the deficiencies in the prior art, the object of the present invention is to provide a decolorization method of Sapindus sapinsin, which overcomes the problems of high target product loss rate, poor decolorization effect, high cost, and environmental pollution in traditional decolorization methods.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Weigh 6g of dried Sapindus saponin powder, add 100mL of pure water, stir at room temperature to dissolve completely; use hydrochloric acid to adjust the pH of the dissolved Sapindus saponin solution to 4.5, add potassium borohydride and sulfurous acid 60 mg of composite decolorizing agent prepared with sodium hydrogen at a mass ratio of 4:3, and reduced and decolorized at 20°C for 80 minutes; then spray-dried the above-mentioned decolorized Sapindus chinensis solution to obtain decolorized Sapindus sapindus saponin powder.

Embodiment 2

[0027] Weigh 12g of dried Sapindus saponin powder, add 200mL of pure water, stir at room temperature to make it completely dissolved; use sulfuric acid to adjust the pH of the dissolved Sapindus saponin solution to 5.0, add sodium borohydride and sulfurous acid Prepare 90 mg of compound decolorizing agent with sodium hydrogen at a mass ratio of 3:2, and reduce and decolorize it at 30°C for 70 minutes; then spray-dry the above-mentioned decolorized Sapinberry solution to obtain decolorized Sapinberry saponin powder.

Embodiment 3

[0029] Weigh 18g of dried Sapindus saponin powder, add 300mL of pure water, stir at room temperature to make it completely dissolved; use hydrochloric acid to adjust the pH of the dissolved Sapindus saponin solution to 5.5, add potassium borohydride and sulfurous acid 120 mg of composite decolorizing agent prepared with sodium hydrogen at a mass ratio of 1:5, and reduced and decolorized at 40°C for 60 minutes; then spray-dried the above-mentioned decolorized Sapinberry solution to obtain decolorized Sapinberry saponin powder.

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Abstract

A method for decolorizing sapindus saponin, comprising the following steps: (1) weighing dried sapindus saponin powder, adding 0.6 times the quality of deionized water, stirring at room temperature to completely dissolve it; (2) by Metal complex hydrides and acidic sulfites are mixed in a mass ratio of 4:3 to 4:36 to prepare a composite decolorizer; (3) after adjusting the pH of the sapindus saponin solution in step (1) to 4.5-6.5 , add the compound decolorizing agent prepared in step (2), the addition amount is weighed according to the mass ratio of Sapindus sapinsin powder and compound decolorizing agent 100:1~100:5, and reduce and decolorize at a temperature of 20°C-70°C for 30 ‑80min; (4) Spray-dry the Sapindus Sapindus total saponins solution after decolorization in step (3) to obtain decolorized saponin powder. The composite decolorizing agent of the present invention has a synergistic effect, less decolorizing agent dosage, good decolorizing effect, short decolorizing time, low production cost, less impact of waste liquid on the environment, less target product loss in the decolorizing process, high efficiency, time saving, The advantages of environmental protection.

Description

technical field [0001] The invention belongs to the technical field of biochemical research, and in particular provides a method for decolorizing the total sapindoside extract of sapindus chinensis. Background technique [0002] Sapindus mukorossi Gaertn. is a deciduous tree of the genus Sapindus L. in the family Sapindaceae, commonly known as Sapindus mukorossi Gaertn., soap tree, etc. It is mainly distributed in the warmer regions of America, Asia and Oceania. It is mainly produced in the Huaihe River Basin and south of my country. The fruits and roots of Sapindus chinensis are rich in sapindus saponins, oil compounds and a small amount of flavonoids, alkaloids, steroids and other secondary metabolites, as well as rich trace elements and proteins. Soapberry saponins are mainly triterpene saponins and sesquiterpene glycosides. Currently, more than 50 species of triterpene saponins and more than 10 species of sesquiterpenes have been identified. Sapindus saponins not only ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07G3/00C07H1/06C07H15/256C07J63/00
CPCC07G3/00C07H1/06C07H15/256C07J63/008
Inventor 邹峥嵘邓宝琴
Owner JIANGXI NORMAL UNIV
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