A kind of natural antiseptic, preparation method thereof and application in cosmetics
A technology of natural preservatives and shallots, applied in the field of natural preservatives and their preparation, can solve the problems of hard to achieve the claimed effect of preservatives, high price, affecting smell and color, etc.
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Embodiment 1
[0048] (1) Enzymolysis treatment of compound plants
[0049] Grinding and pulverizing 8 parts by mass of Iridaceae shallots and 1 part by mass of thyme root after being air-dried at 85°C for 4 hours to 80 mesh, and then adding 54 parts by mass of water to the reaction kettle, adding 0.00225 parts by mass of cellulase (purchased From Novozymes, brand name: Celluclast 1.5L, enzyme activity: 700EGU / ml, the same below) and 0.00225 parts by mass of pectinase (purchased from Novozymes, brand name: Pectinex BE XXL, enzyme activity: 16000PECTU / ml, the same below), the pH was adjusted to 6.8 with triethanolamine, and the enzyme was hydrolyzed at 65°C for 2h. Centrifuge after the post-treatment, and air-dry the filter cake at 85° C. for 4 hours to obtain 8.5 parts by mass of Irisaceae red onion and thyme root powder in total, with a water content of 0.2%.
[0050] (II) Subcritical Extraction of Compound Plants
[0051] Add 8.5 parts by mass of the powder obtained in step (I) into a su...
Embodiment 2
[0055] (1) Enzymolysis treatment of compound plants
[0056] Grind and pulverize 9 parts by mass of Iridaceae red onion and 1 part by mass of thyme root after air drying at 85°C for 6 hours to 90 mesh, then add 80 parts by mass of water to the reaction kettle, add 0.006 parts by mass of cellulase and 0.004 parts by mass of A compound enzyme composed of parts by mass of pectinase is used to adjust the pH to 7.2 with sodium hydroxide, and the enzyme is hydrolyzed at 70° C. for 3 hours. Centrifuge after the post-treatment, and air-dry the filter cake at 85° C. for 5 hours to obtain 9.5 parts by mass of treated Iridaceae red onion and thyme root powder, with a water content of 0.12%.
[0057] (II) Subcritical Extraction of Compound Plants
[0058] Add 9.5 parts by mass of the powder obtained in step (I) into a subcritical extraction tank, pass through the subcritical fluid butane to extract 3 times at 40°C and 0.5MPa, and the extraction time is 30min; after the extraction is comp...
Embodiment 3
[0062] (1) Enzymolysis treatment of compound plants
[0063] Grind and pulverize 10 parts by mass of Iridaceae red onion and 1 part by mass of thyme root after air drying at 85°C for 6 hours to 100 mesh, then add 99 parts by mass of water to the reaction kettle, add 0.0147 parts by mass of cellulase and 0.0073 parts by mass of A compound enzyme composed of pectinase in parts by mass, adjusted to pH 7.5 with potassium hydroxide, and hydrolyzed at 75° C. for 4 hours. Centrifuge after the post-treatment, and air-dry the filter cake at 85° C. for 6 hours to obtain 10.4 parts by mass of Irisaceae red onion and thyme root powder in total, with a water content of 0.1%.
[0064] (II) Subcritical Extraction of Compound Plants
[0065] Add 10.4 parts by mass of the powder obtained in step (I) into a subcritical extraction tank, pass through the subcritical fluid butane to extract 4 times at 45°C and 0.8MPa, and the extraction time is 40min; after the extraction is completed, analyze at...
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