Preparation method and application of carbon nanofiber, tin disulfide, tin dioxide and sulfur composite material with heterojunction structure
A technology of carbon nanofiber and tin disulfide, which is applied in the direction of nanotechnology, nanotechnology, structural parts, etc. for materials and surface science, can solve problems such as lithium polysulfide shuttle effect, and achieve clean and environmentally friendly preparation process and high production process Simple, transformative effect
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specific Embodiment approach 1
[0021] Specific embodiment one: what this embodiment records is a kind of preparation method of carbon nanofiber, tin disulfide, tin dioxide and sulfur composite material with heterojunction structure, described method steps are as follows:
[0022] Step 1: Dissolve 16 mg of thioacetamide and 32-80 mg of tin tetrachloride in 10 mL of isopropanol, add carbon nanofibers with a diameter of 1 cm, react in hydrothermal reaction at 180 ° C for 24 hours, and cool naturally to room temperature. Dry overnight at a temperature of 70°C to obtain a carbon nanofiber, tin disulfide and tin dioxide composite material with a heterojunction structure;
[0023] Step 2: Dissolve 200-400 mg of sulfur powder in 5 mL of carbon disulfide to obtain a sulfur solution, and impregnate the carbon nanofibers, tin disulfide and tin dioxide composite materials with a heterojunction structure in step 1 into the sulfur solution to make the sulfur The loading capacity is 1.5-3.0mg cm -2 After 5 minutes, it wa...
specific Embodiment approach 2
[0024] Specific embodiment two: a method for preparing a carbon nanofiber, tin disulfide, tin dioxide and sulfur composite material with a heterojunction structure described in specific embodiment one, the carbon nanofiber, tin disulfide and disulfide The morphology of tin oxide is a nanosheet array structure with a rough surface.
specific Embodiment approach 3
[0025] Embodiment 3: Application of the carbon nanofiber, tin disulfide, tin dioxide and sulfur composite material prepared by the method described in Embodiment 1 or 2 in the positive electrode of lithium-sulfur battery.
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