Preparation method of Jun porcelain with natural cracks
A preparation process and natural crack technology, which is applied in the field of Jun porcelain preparation technology with natural cracks, can solve the problems of difficult firing, complicated production process, and low rate of Jun porcelain treasures, and achieve the effect of preventing shedding
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Embodiment 1
[0032] Step 1. Put the dried green body into the kiln for firing. When the firing temperature rises to 550°C, close the kiln door, and stop the fire when the temperature continues to rise to 980°C. The heating rate at this stage is 20-2°C / min, take it out after cooling, and get the plain tire;
[0033] Step 2: Attach a layer of 0.1cm-thick green body slurry on the surface of the plain body, and then put it into the kiln again for secondary firing. When the temperature is 550°C, the heating rate is 12-1°C / min. When the temperature rises to 980°C, the heating rate is 5°C. At this time, the heating rate should not be too fast to prevent the outer layer of the green body from falling off;
[0034] Step 3. When the plain embryo after the secondary firing is cooled to 190°C, it is taken out and placed in a constant temperature and pressure container with a pressure of 200MPa and a temperature of 80°C. After being kept warm for 1 hour, it is taken out and naturally cooled to room te...
Embodiment 2
[0045] Step 1. Put the dried green body into the kiln for firing. When the firing temperature rises to 575°C, close the kiln door, and stop the fire when the temperature continues to rise to 990°C. The heating rate at this stage is 21°C / min. Take it out after cooling to get plain tires;
[0046] Step 2: Attach a layer of 0.15cm-thick green body slurry on the surface of the plain body, and then put it into the kiln again for secondary firing. When the temperature is 575°C, the heating rate is 13°C / min, and the temperature rises When the heating rate is as high as 990°C, the heating rate is 6°C. At this time, the heating rate should not be too fast, so as to avoid the outer layer of the green body from falling off;
[0047] Step 3. When the plain embryo after the secondary firing is cooled to 195°C, it is taken out and placed in a container with a pressure of 200MPa and a temperature of 90°C. After being kept warm for 1.5 hours, it is taken out, and naturally cooled to room temp...
Embodiment 3
[0058] Step 1. Put the dried biscuit into the kiln for firing. Close the kiln door when the firing temperature rises to 600°C, and stop the fire when the temperature continues to rise to 1000°C. The heating rate at this stage is 22°C / min. Take it out after cooling to get plain tires;
[0059] Step 2: Attach a layer of 0.2cm-thick green body slurry on the surface of the plain tire, and then put it into the kiln again for secondary firing. When the temperature is 600°C, the heating rate is 14°C / min, and the temperature rises The temperature rise rate is 7°C when the temperature is as high as 1000°C. At this time, the temperature rise rate should not be too fast to avoid the outer layer of the green body from falling off;
[0060] Step 3. When the plain embryo after the secondary firing is cooled to 200°C, take it out and place it in a container with a pressure of 200MPa and a temperature of 100°C, take it out after keeping it warm for 2 hours, and cool it naturally to room tempe...
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