Preparation method of incomplete dehydrated magnesium chloride snow-melting agent
A technology of magnesium chloride and snow melting agent, applied in magnesium chloride, chemical instruments and methods, magnesium halide and other directions, can solve the problems of polluting the ecological environment of the salt lake, restricting the sustainable development of the salt lake potash fertilizer industry, complicated preparation process, etc. The effect of promoting sustainable development and low preparation cost
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Embodiment 1
[0017] This example provides a preparation method of an incompletely dehydrated magnesium chloride deicing agent. The incompletely dehydrated magnesium chloride deicing agent uses bischofite as a by-product of the salt lake as a raw material, and can make full use of this part of by-products, not only turning waste into treasure , save resources, and avoid pollution of the salt lake ecological environment, and provide guarantee for the sustainable development of the salt lake potash industry.
[0018] The preparation method of the incompletely dehydrated magnesium chloride deicing agent according to this embodiment includes the following steps: dehydrating the bischofite by-product of the salt lake in a fluidized equipment at 50°C to 70°C to obtain the first incompletely dehydrated Magnesium chloride deicing agent.
[0019] Specifically, the incompletely dehydrated magnesium chloride in the obtained first incompletely dehydrated magnesium chloride deicing agent has 4 to 6 crys...
Embodiment 2
[0026] In the description of Embodiment 2, the similarities with Embodiment 1 will not be repeated here, and only the differences with Embodiment 1 will be described. The difference between embodiment 2 and embodiment 1 is that in the process of preparing the incomplete dehydration magnesium chloride deicing agent in embodiment 2, the first incomplete dehydration magnesium chloride deicing agent obtained in embodiment 1 must continue to be fluidized Two-stage dehydration is carried out in the bed at 100°C to 130°C, thereby obtaining a second incompletely dehydrated magnesium chloride deicing agent; the incompletely dehydrated magnesium chloride in the second incompletely dehydrated magnesium chloride deicing agent has 3 to 4 crystal waters.
[0027] It is worth noting that, in the process of changing from the first incompletely dehydrated magnesium chloride deicing agent to the second incompletely dehydrated magnesium chloride deicing agent, the bed area of the fluidized bed,...
Embodiment 3
[0030] In the description of Embodiment 3, the similarities with Embodiment 2 will not be repeated here, and only the differences with Embodiment 2 will be described. The difference between embodiment 3 and embodiment 2 is that in the process of preparing the incomplete dehydration magnesium chloride deicing agent in embodiment 3, the second incomplete dehydration magnesium chloride deicing agent obtained in embodiment 2 must be continued in fluidization Three stages of dehydration are carried out in the bed at 150°C to 180°C, thereby obtaining a third incompletely dehydrated magnesium chloride deicing agent; the incompletely dehydrated magnesium chloride in the third incompletely dehydrated magnesium chloride deicing agent has 2 to 3 crystal waters.
[0031] In this embodiment, in the process of changing from the second incompletely dehydrated magnesium chloride deicing agent to the third incompletely dehydrated magnesium chloride deicing agent, the bed area, feed amount, dehy...
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