Novel floatable solid foam scrubbing rod and preparation method thereof
A new type of foam discharge rod technology, which is applied in chemical instruments and methods, mining fluids, earthwork drilling, etc., can solve the problems of slow dissolution speed, small contact surface, shortening the dissolution time of foam discharge rods, etc., and achieves a simple and easy preparation method. It has the effect of improving foam stability and good compatibility.
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Embodiment 1
[0046] In this example, the components and proportions of several floating solid bubble bars are given, and the preparation methods of each bubble bar are given.
[0047] (1) Floatable solid bubble row stick SRP-1
[0048] The components and their ratios are: 50 kg of dodecyl ethoxy sulfobetaine, 15 kg of coconut monoethanolamide, 10 kg of thiourea, 5 kg of sodium chloride, 3 kg of polyvinyl alcohol, and 2 kg of sodium benzoate.
[0049] The preparation method of floating solid bubble stick SRP-1:
[0050] Step 1: Put 50 kg of dodecyl ethoxy sulfobetaine, 15 kg of coco-monoethanolamide, and 10 kg of thiourea into a container. After mixing, heat to 50° C., heat and dry for 3 hours.
[0051] Step 2: Then add 5 kg of sodium chloride, 3 kg of polyvinyl alcohol, and 2 kg of sodium benzoate to the container of step 1, mix well, start heating, gradually increase the temperature to 80°C, keep it for 5 hours until the material is dried;
[0052] Step 3: After the material obtained in step 2 is co...
Embodiment 2
[0078] The above-mentioned floating solid foam sticks SRP-1, SRP-2, SRP-3, SRP-4, SRP-5 were prepared according to the preparation method described in Example 1 to prepare foam sticks. For the structure of these bubble bars, see Figure 1 to Figure 4 .
[0079] Such as figure 1 with 4 As shown, this embodiment provides a floating bubble row rod for gas production in an oil and gas field. In terms of overall shape, the bubble bar is similar to the existing bubble bar, and both are cylindrical rods 1 made of a bubble bar. The difference is that the two ends of the bubble bar in this embodiment are provided with arc-shaped transition sections 2, and the surfaces of the cylindrical rod body 1 and the arc-shaped transition section 2 are provided with threads 4. It should be noted that the cylindrical rod body 1 and the arc-shaped transition sections 2 at both ends thereof are an integral structure.
[0080] In this embodiment, the curvature of the arc-shaped transition section 2 conne...
Embodiment 3
[0084] In this example, the performance of the floatable solid bubble bar SRP-1, SRP-2, SRP-3, SRP-4, and SRP-5 was tested and compared with the performance of the commercially available bubble bar UT-6. Design performance test according to industry standard SY / T5761-1995. The preparation of different concentrations of mineralized water used in this embodiment is as follows.
[0085] Industry standard water type: weigh 12.5g NaCl and 2.5g CaCl 2 Dissolve it in a clean small beaker, then pour it into a 250ml volumetric flask to make a constant volume, and make a 60g / L salinity aqueous solution.
[0086] NaHCO 3 Water type: weigh 1.25g NaHCO 3 Dissolve it in a small clean beaker, then pour it into a 250ml volumetric flask to make a constant volume and prepare a 5g / L salinity aqueous solution.
[0087] CaCl 2 Water type: weigh 15g NaCl and 27.5g CaCl 2 Dissolve it in a clean small beaker, then pour it into a 250ml volumetric flask to make a constant volume, and make it into an aqueous ...
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