In-situ micro-glass-fiber reinforced polymer based 3D printing consumables as well as preparation method and equipment thereof
A 3D printing and polymer technology, applied in the field of material science, to achieve the effect of easy continuous production, easy large-scale production, and improved mechanical properties
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Embodiment 1
[0013] Example 1 of the present invention: in-situ micro glass fiber reinforced polymer 3D printing consumables, calculated by mass parts, including 80 parts of PLA, 18 parts of phosphate glass-ceramic and 5502 parts of silane coupling agent Kh. Phosphate glass-ceramic is prepared by firing stannous chloride and ammonium dihydrogen phosphate at a mass percentage of 1:1 at 500°C for 25 minutes, and its glass transition temperature is 215°C.
[0014] The preparation method of in-situ micro-glass fiber reinforced polymer 3D printing consumables, each component is taken according to the above-mentioned mass parts, and the polymer matrix, phosphate glass-ceramic and coupling agent are premixed evenly, and then reinforced with in-situ glass fiber Polymer 3D printing consumables production equipment is extruded, and after extrusion, after stretching, cooling, and winding processes, in-situ micro-glass fiber reinforced polymer 3D printing consumables are prepared.
[0015] In-situ gla...
Embodiment 2
[0017] Example 2 of the present invention: in-situ micro glass fiber reinforced polymer 3D printing consumables, calculated by mass parts, including 84 parts of EVA, 15 parts of phosphate glass-ceramic and 1 part of titanate coupling agent KR101. Phosphate glass-ceramic is prepared by firing stannous chloride and ammonium dihydrogen phosphate at a mass percentage of 1:1 at 500°C for 25 minutes, and its glass transition temperature is 215°C.
[0018] The preparation method and production equipment are the same as in Example 1.
[0019] In order to verify the effect of the present invention, the mechanical properties of the in-situ micro glass fiber reinforced polymer 3D printing consumables prepared by the above implementation examples were tested for mechanical properties, and the results are shown in the following table:
[0020]
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