Natural mildew-proof and corrosion-proof agent for bamboos and woods
A preservative and wood technology, applied in the direction of impregnating wood, wood impregnation, wood processing appliances, etc., can solve the problems of human harm, mildew-proof and preservative toxicity, etc., and achieve the effect of strong anti-loss and long-term mildew-proof effect.
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Embodiment 1
[0018] The production method of Ginkgo biloba extract: (1) Drying and crushing: Fresh ginkgo fruits are removed from the ginkgo biloba to obtain the testa, dried in a vacuum drying oven at 65°C to a moisture content of 4.65%, and crushed until most of the particles pass 50 mesh Sieve; (2) Extraction: use 70% ethanol solution as the extraction liquid, and carry out extraction according to the material-to-liquid ratio (material weight / solution weight) 1:5, and the extraction time is 5 hours; during the extraction process, ultrasonic treatment 4 30 minutes each time; (3) Purification: filter the extract to obtain the filtrate, add 0.1 mol / L acetic acid to the filtrate, adjust the pH to 3.0, extract 4 times with ethyl acetate, and separate ethyl acetate Ester phase; (4) Concentration: The ethyl acetate phase was subjected to rotary steaming at 75°C to obtain the Ginkgo biloba exocarp extract.
[0019] With reference to the raw materials and parts by weight of Example 1 in the above t...
Embodiment 2
[0021] Production method of Ginkgo biloba extract: (1) Drying and crushing: Fresh ginkgo fruits are removed from the ginkgo fruit to obtain the extrus, dried in a vacuum drying oven at 65°C to a moisture content of 4.28%, and crushed until most of the particles pass 50 mesh Sieve; (2) Extraction: use 50% ethanol solution as the extraction liquid, and carry out extraction according to the material-to-liquid ratio (material weight / solution weight) 1:10, and the extraction time is 3 hours; during the extraction process, ultrasonic treatment 3 20 minutes each time; (3) Purification: filter the extract to obtain the filtrate, add 0.1 mol / L acetic acid to the filtrate, adjust the pH to 3.5, and extract 3 times with ethyl acetate to separate ethyl acetate Ester phase; (4) Concentration: The ethyl acetate phase was subjected to rotary steaming at 70°C to obtain the Ginkgo biloba exocarp extract.
[0022] With reference to the raw materials and parts by weight of Example 2 in the above ta...
Embodiment 3
[0024] The production method of Ginkgo biloba exocarp extract: (1) Same as Example 1; (2) Extraction: 30% ethanol solution is used as the extraction liquid, and the material-to-liquid ratio (material weight / solution weight) is 1:5 for extraction , The extraction time is 2 hours; during the extraction process, ultrasonic treatment is performed twice, each time is 15 minutes; (3) purification: the extraction liquid is filtered to obtain the filtrate, and 0.1 mol / L acetic acid is added to the filtrate to adjust the pH value To 3, extract twice with ethyl acetate, and separate the ethyl acetate phase; (4) Concentration: the ethyl acetate phase is rotary evaporated at 70°C to obtain the Ginkgo biloba exocarp extract.
[0025] With reference to the raw materials and parts by weight of Example 3 in the above table, first add 5 parts of Ginkgo biloba exocarp extract to 105 parts of dissolving agent (ethanol to water ratio 5:5), and slowly add 0.5 part of chitosan after it is completely di...
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