AIN-doped modified visible-light activity photocatalyst preparation method
A photocatalyst and visible light technology, applied in the field of air purification, can solve the problems of insignificant photocatalyst modification effect, narrowing the use range of photocatalyst, and low utilization rate of sunlight, and achieve excellent effect, narrow energy level gap, and good photocatalytic activity. Effect
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Embodiment 1
[0024] The preparation method of AlN-doped modified visible light active photocatalyst, the specific steps are first taking 10ml of nano-TiO with a solid content of 10%. 2 Colloidal solution, diluted 1:9 with deionized water to form nano-TiO 2 Colloid dilute solution, this is the photocatalyst solution; then, add nano-aluminum nitride of 0.01wt% of photocatalyst solution weight to the photocatalyst solution to carry out doping modification, stir 0.5h under the condition of 250rpm, finally, obtain the photocatalyst solution of modification .
[0025] Spray the prepared modified photocatalyst evenly on a 200*250mm glass sheet, then place it in a closed transparent glass reaction vessel to investigate the visible light activity of the modified photocatalyst, select a 20W incandescent lamp to simulate sunlight, and inject it into the reaction vessel 5ppm of formaldehyde gas, the degradation product of formaldehyde CO 2 Generate speed and concentration to characterize the visible...
Embodiment 2
[0027] The preparation method of AlN-doped modified visible light active photocatalyst, the specific steps are first taking 10ml of nano-TiO with a solid content of 10%. 2 Colloidal solution, diluted 1:9 with pure water to form nano-TiO 2 The dilute colloidal solution, which is the photocatalyst solution; then, doping and modifying the photocatalyst solution with 0.1% nano-AlN by weight of the photocatalyst solution, stirring at 250rpm for 0.5h, and finally obtaining the modified photocatalyst solution.
[0028] Spray the prepared modified photocatalyst evenly on a 200*250mm glass sheet, then place it in a closed transparent glass reaction vessel to investigate the visible light activity of the modified photocatalyst, select a 20W incandescent lamp to simulate sunlight, and inject it into the reaction vessel 5ppm of ethanol gas, the degradation product of ethanol CO 2 Generate speed and concentration to characterize the visible light activity of the modified photocatalyst, th...
Embodiment 3
[0030] With above-mentioned embodiment 1, its difference is:
[0031] Nano TiO in step (1) 2 The solid content of the colloidal solution is 15wt%, and the surface potential is 37mV; Nano TiO 2 The solid content of the dilute solution is 0.5wt%.
[0032] In the step (2), the average particle size of the nano-aluminum nitride is 45nm, and the addition amount is 0.05wt% of the weight of the photocatalyst solution; the stirring speed is 300rpm, and the stirring time is 1h.
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