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Resistive macromolecule humidity-sensitive material and preparation method thereof

A moisture-sensitive material, resistance-type technology, applied in the analysis of materials, material analysis through electromagnetic means, material resistance, etc., can solve problems such as hindering popularization and application, poor high-humidity resistance and long-term stability, and easy slip loss. Achieve good humidity response, high humidity resistance and long-term stability, and improve water resistance

Active Publication Date: 2017-02-01
GUANGZHOU AOSONG ELECTRONIC CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this type of sensor mostly uses traditional linear polymer electrolytes as sensitive materials, which are prone to slip and loss in high-humidity environments. As the humidity increases, the polymer materials will absorb moisture and expand, resulting in their high-humidity resistance and long-term Poor stability hinders its further popularization and application to a certain extent

Method used

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  • Resistive macromolecule humidity-sensitive material and preparation method thereof
  • Resistive macromolecule humidity-sensitive material and preparation method thereof
  • Resistive macromolecule humidity-sensitive material and preparation method thereof

Examples

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Effect test

Embodiment 1

[0037] Take 20 parts of acryloyloxyethyltrimethylammonium chloride, 10 parts of acrylamide, 10 parts of methyl methacrylate, 2 parts of lithium acrylate, and 0.5 parts of initiator AIBN, and place it in a Add methanol to the four-necked flask of the condenser tube and the nitrogen protection device to completely dissolve the reactants, and then react at a constant temperature of 65-85° C. for 4 hours. After the reaction is finished, the obtained product is washed with ether, and then vacuum-dried at room temperature to obtain a resistive polymer moisture-sensitive material.

Embodiment 2

[0039] Take 20 parts of methacryloyloxyethyltrimethylammonium chloride, 40 parts of diethylaminoethyl methacrylate, 10 parts of styrene, 2 parts of sodium styrene sulfonate, 1 part of initiator AIBN, and place in a Methanol was added to a four-necked flask with a thermometer, a stirrer, a reflux condenser and a nitrogen protection device to completely dissolve the reactant, and then reacted at a constant temperature of 65-85° C. for 6 hours. After the reaction, the obtained product was washed with ether and dried in vacuum at room temperature to obtain a resistive polymer moisture-sensitive material.

Embodiment 3

[0041] Take 20 parts of methacryloylpropyltrimethylammonium chloride, 20 parts of dimethyl allylamine, 10 parts of methyl acrylate, 5 parts of sodium styrene sulfonate, and 0.8 parts of initiator AIBN, and put them in the Add methanol to a four-necked flask equipped with a thermometer, a stirrer, a reflux condenser and a nitrogen protection device to completely dissolve the reactants, and then react at a constant temperature of 65-85° C. for 6 hours. After the reaction, the obtained product was washed with ether and dried in vacuum at room temperature to obtain a resistive polymer moisture-sensitive material.

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Abstract

The invention discloses a resistive macromolecule humidity-sensitive material. A component A, a component B, a component C and a component D react to generate the humidity-sensitive material in a polymerization manner, the component A is one of acryloyloxyethyl trimethyl ammonium chloride, methylacryloyl propyl trimethyl ammonium chloride, methylacrylylethyl trimethyl ammonium chloride; the component B is one of N-methyl allyl amine, acrylamide, dimethylallylamine, dimethylaminoethyl methacrylate, diethyl-amino-ethylmethacrylate and dimethylaminoethyl acrylate; the component C is one of methyl methacrylate, butyl methacrylate, methyl acrylate, butyl acrylate, styrene and ethenylmethyl benzene; the component D is one of sodium p-styrenesulfonate and lithium acrylate. The resistive macromolecule humidity-sensitive material is good in high-humidity resistance and long-term stability.

Description

technical field [0001] The invention relates to a polymer material, in particular to a polymer material with humidity sensitive resistance properties and a preparation method thereof. Background technique [0002] Currently commercialized humidity sensors mainly include inorganic ceramic semiconductor type and organic polymer type. The polymer humidity sensor has become the mainstream of the humidity sensor because of its good response characteristics, wide measurement range, good stability, room temperature detection, easy integration, miniaturized mass production, and low price. Among them, the polymer resistive humidity sensor is very simple to prepare, has good performance, and is easy to integrate into the system to realize the measurement and control of humidity. It is one of the research and development of humidity sensors. However, this type of sensor mostly uses traditional linear polymer electrolytes as sensitive materials, which are prone to slip and loss in high...

Claims

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Application Information

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IPC IPC(8): C08F220/34C08F220/56C08F220/14C08F220/06C08F212/08C08F212/14C08F226/02C08F220/18C09D133/14C09D7/12G01N27/04
CPCG01N27/048C09D133/14C08F220/34C08F226/02C08K5/02C08F220/1804C08F220/06C08F220/14C08F212/14C08F212/08C08F220/56
Inventor 张宾
Owner GUANGZHOU AOSONG ELECTRONIC CO LTD
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