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Preparation method of weather-resistance tile adhesion agent for exterior wall ceramic tiles

A tile adhesive and weather-resistant technology, which is applied in the field of preparation of weather-resistant tile adhesive for exterior wall tiles, can solve the problems of weak adhesion between tiles and walls, being susceptible to sudden temperature changes, and tile peeling. Achieve the effect of low production cost, simple preparation steps and enhanced adhesion

Inactive Publication Date: 2017-02-01
郭舒洋
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved by the present invention: Aiming at the disadvantages of poor weather resistance of current tile adhesives and being easily affected by sudden temperature changes, resulting in weakened bonding force between tiles and walls, cracking and peeling of tiles, a method of using saturated adhesives is provided. Water vapor pressurization treatment hydrolyzes the acetyl group contained in bagasse cellulose to generate acetic acid. Under acidic environmental conditions, the cellulose and hemicellulose in the material decompose, and then rapidly reduce the pressure to make the fiber instantly expand and break down. Then freeze with liquid nitrogen to make ice crystals between the bagasse fibers, break the ice crystals under the pressure of ball milling to form bagasse fiber whiskers, mix with nano silicon dioxide, and carbonize under nitrogen atmosphere to carbonize the bagasse fiber whiskers Finally, silicon carbide whiskers are grown on the surface, and modified bagasse whiskers are prepared as a reinforcing agent, and then the glutinous rice is boiled and beaten into a slurry as a binder, mixed with Portland cement, etc., and ball milled to obtain a weather-resistant tile for exterior walls. Type ceramic tile adhesive, the present invention effectively solves the problem of its poor weather resistance and weakens the bonding force between tiles and walls by adding self-prepared whiskers as added fibers

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0018] First, weigh 3kg of bagasse, pour it into a high-pressure reactor, and feed saturated steam into the reactor at a stirring speed of 350r / min and a temperature of 95°C until the pressure in the reactor reaches 3.5MPa. After 10 minutes, open the discharge valve at the bottom of the reaction kettle, so that the materials in the reaction kettle are sprayed into the receiving kettle; after the materials in the receiving kettle are naturally cooled to room temperature, the materials are transferred to a liquid nitrogen freezer, frozen with liquid nitrogen for 2 minutes, and then quickly Pour the frozen material into the ball mill, add zirconia ball milling beads according to the ball-to-material ratio of 30:1, mill for 15 minutes, collect the ball-milled material, transfer it to a vacuum drying oven, and dry it at a temperature of 105°C To constant weight, the bagasse fiber whiskers are obtained; then the bagasse fiber whiskers obtained above are mixed with nano-silicon dioxid...

example 2

[0021]First weigh 4kg of bagasse, pour it into a high-pressure reactor, and at a stirring speed of 375r / min and a temperature of 100°C, feed saturated steam into the reactor until the pressure in the reactor reaches 3.8MPa, and keep the pressure After 13 minutes, open the discharge valve at the bottom of the reaction kettle, so that the materials in the reaction kettle are sprayed into the receiving kettle; after the materials in the receiving kettle are naturally cooled to room temperature, the materials are transferred to a liquid nitrogen freezer and treated with liquid nitrogen for 3 minutes, and then quickly Pour the frozen material into a ball mill, add zirconia ball milling beads according to the ball-to-material ratio of 35:1, and mill for 18 minutes. Collect the ball-milled material, transfer it to a vacuum drying oven, and dry it at a temperature of 108°C. To constant weight, the bagasse fiber whiskers are obtained; then the above-mentioned bagasse fiber whiskers and ...

example 3

[0024] First weigh 5kg of bagasse, pour it into a high-pressure reactor, and feed saturated steam into the reactor at a stirring speed of 400r / min and a temperature of 105°C until the pressure in the reactor reaches 4.0MPa. After 15 minutes, open the discharge valve at the bottom of the reaction kettle, so that the materials in the reaction kettle are sprayed into the receiving kettle; after the materials in the receiving kettle are naturally cooled to room temperature, the materials are transferred to a liquid nitrogen freezer and treated with liquid nitrogen for 4 minutes, and then quickly Pour the frozen material into the ball mill, add zirconia ball milling beads according to the ball-to-material ratio of 40:1, mill for 20 minutes, collect the ball-milled material, transfer it to a vacuum drying oven, and dry it at a temperature of 110°C To constant weight, the bagasse fiber whiskers are obtained; then the bagasse fiber whiskers obtained above are mixed with nano-silicon di...

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Abstract

The invention discloses a preparation method for a weather-resistance tile adhesion agent for exterior wall ceramic tiles, and belongs to the technical field of tile adhesion agent preparation. The preparation method comprises the steps that a pressure treatment is conducted with saturated steam, so that acetic acid is formed by hydrolysis of ethanoyl contained in bagasse cellulose, under the condition of acid environment, the cellulose and hemicellulose in the materials are disintegrated, then the pressure is released rapidly, the cellulose is instantaneously swelled, broken and hydrolyzed, then is frozen with liquid nitrogen, and thus ice crystals are produced among the bagasse cellulose; the ice crystals are burst by ball milling, and thus bagasse cellulose whisker is formed; the bagasse cellulose whisker is mixed with nanosilicon dioxide for carbonization under nitrogen atmosphere, after the bagasse cellulose whisker is carbonized, silicon carbide whisker is grown on the surface of the bagasse cellulose whisker, and the modified bagasse whisker is prepared as a reinforcing agent, moreover, sticky rice is cooked and beaten into a pulp liquid as an adhesion agent; the reinforcing agent, the adhesion agent and portland cement are mixed and are subjected to ball milling, then the weather-resistance tile adhesion agent for the exterior wall ceramic tiles is prepared. The preparation method has the advantages that the prepared product has good weather resistance, and is free of cracks and tile spalling after use.

Description

technical field [0001] The invention relates to a preparation method of a weather-resistant tile adhesive for exterior wall tiles, and belongs to the technical field of tile adhesive preparation. Background technique [0002] The rapid development of architectural ceramics has made a significant contribution to the beautification of cities and home environments. The traditional tile paste method mostly uses cement mortar, which is to mix sand and cement on site to make simple cement mortar, apply this mortar on the back of pre-soaked or pre-wetted tiles, and press the mortar-coated tiles onto the pre-wetted surface on the tile, then tap the tile to ensure a consistent flatness of the tile. The main purpose is to compact the mortar so that the cement particles get into the interior of the porous back of the tile and into the porous substrate. The disadvantages of this kind of mortar are weak cohesion, poor durability, easy to peel off, and large amount of construction mater...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B28/04C04B20/04C04B111/20
CPCC04B28/04C04B20/04C04B2111/00637C04B2111/20C04B18/248C04B24/00C04B14/28C04B18/08C04B14/042C04B24/283C04B20/026C04B20/023C04B14/06
Inventor 郭舒洋邹宇帆许洪祥
Owner 郭舒洋
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