A kind of highly transparent and antifouling coating solution and preparation method thereof
A coating solution and high-transparency technology, applied in antifouling/underwater coatings, biocide-containing paints, coatings, etc., can solve the problems of poor dirt resistance, high surface activity, and easy entry of films, and achieve improved Anti-fouling ability, reduced surface activity, good anti-fouling effect
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Embodiment 1
[0027] A high-transparency anti-fouling coating solution and a preparation method thereof, comprising the following steps:
[0028] A. Film-forming substance solution: in parts by weight, mix 4 parts of ethyl orthosilicate, 12 parts of isopropanol, 2.3 parts of KH560, and 1.5 parts of phenyltrimethoxysilane in order, stir for 60 minutes, add the mixed Acid solution (pure water and 37% concentrated hydrochloric acid are 1 part and 0.03 part respectively), stirred and heated to 60 ° C, the reaction time is 8 hours, cooled to room temperature and aged for 24 hours;
[0029] B. Sealing substance solution: mix 8 parts of propylene glycol methyl ether, 1 part of polyether-modified polysiloxane, and 2 parts of polyethylene glycol in parts by weight at room temperature, stir for 30 minutes, and then let stand 1h;
[0030] C. Pore-forming substance solution: in parts by weight, 1 part of methacrylic resin stock solution is evenly dispersed in 5 parts of isopropanol, stirred for 30 min...
Embodiment 2
[0033] A high-transparency anti-fouling coating solution and a preparation method thereof, comprising the following steps:
[0034] A. Film-forming substance solution: in parts by weight, mix 5 parts of ethyl orthosilicate, 15 parts of isopropanol, 2.4 parts of KH560, and 2.2 parts of phenyltrimethoxysilane in order, stir for 60 minutes, and add the mixed Acid solution (pure water and 37% concentrated hydrochloric acid are 1.4 parts and 0.04 parts respectively), stirred and heated to 80 ° C, the reaction time is 4 hours, cooled to room temperature and aged for 36 hours;
[0035] B. Sealing substance solution: mix 10 parts of propylene glycol methyl ether, 1.5 parts of polyether-modified polysiloxane, and 3 parts of polyethylene glycol in parts by weight at room temperature, stir for 30 minutes, and then let stand 1h;
[0036] C. Pore-forming substance solution: in parts by weight, 1.5 parts of methacrylic resin stock solution was uniformly dispersed in 6 parts of isopropanol,...
Embodiment 3
[0039] A high-transparency anti-fouling coating solution and a preparation method thereof, comprising the following steps:
[0040] A. Film-forming substance solution: in parts by weight, mix 4 parts of ethyl orthosilicate, 12 parts of isopropanol, 2.5 parts of KH570, and 2.1 parts of diphenyldimethoxysilane in order, stir for 60 minutes, add and mix The acid solution (pure water and 37% concentrated hydrochloric acid are 1 part and 0.03 parts respectively), stirred and heated to 80 ° C, the reaction time is 4 hours, cooled to room temperature and aged for 24 hours;
[0041] B. Sealing substance solution: mix 10 parts of propylene glycol methyl ether, 1 part of polyether-modified polysiloxane, and 2 parts of polyethylene glycol in parts by weight at room temperature, stir for 30 minutes, and then let stand 1h;
[0042] C. Pore-forming substance solution: in parts by weight, 1 part of methacrylic resin stock solution is evenly dispersed in 5 parts of isopropanol, stirred for 3...
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