Complex gel fragrance slow release particles and preparation method and application thereof
A technology of composite gel and slow-release granules, applied in application, tobacco, e-liquid filter and other directions, can solve the problems of difficult production and operation control, volatile aroma substances, and complicated process.
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Embodiment 1
[0074] Embodiment 1: Preparation of gel flavor sustained-release granules of the present invention
[0075] The implementation steps of this embodiment are as follows:
[0076] A. Preparation of raw material mixture solution
[0077] 25 parts by weight of β-cyclodextrin, 30 parts by weight of chemically modified starch, 15 parts by weight of hydroxypropyl methylcellulose, 10 parts by weight of sodium carboxymethylcellulose, 5 parts by weight of gellan gum, and 8 parts by weight of gelatin 1. Mix 1 part by weight of chitosan with 1 part by weight of sodium citrate to obtain a powdery material, then add water to the powdery material according to the weight ratio of the powdery material to water as 1:2, stir and mix , dissolving the powdery material to obtain a raw material mixture solution.
[0078] B. Preparation of composite gel
[0079] Heat the polyethylene glycol to a temperature of 45°C to completely melt it, and then mix the melted polyethylene glycol with the raw mate...
Embodiment 2
[0086] Embodiment 2: Preparation of gel flavor sustained-release granules of the present invention
[0087] The implementation steps of this embodiment are as follows:
[0088] A. Preparation of raw material mixture solution
[0089] 30 parts by weight of β-cyclodextrin, 25 parts by weight of bio-modified starch, 18 parts by weight of hydroxypropyl methylcellulose, 6 parts by weight of sodium carboxymethylcellulose, 8 parts by weight of gellan gum, and 7 parts by weight of gelatin 1. Mix 3 parts by weight of chitosan and 2 parts by weight of sodium citrate evenly to obtain a powdery material, then add water to the powdery material according to the weight ratio of the powdery material to water at 1:3, stir and mix , dissolving the powdery material to obtain a raw material mixture solution.
[0090] B. Preparation of composite gel
[0091] Heat the polyethylene glycol to a temperature of 30°C to completely melt it, and then mix the melted polyethylene glycol with the raw mate...
Embodiment 3
[0094] Embodiment 3: Preparation of gel flavor sustained-release granules of the present invention
[0095] The implementation steps of this embodiment are as follows:
[0096] A. Preparation of raw material mixture solution
[0097] 20 parts by weight of β-cyclodextrin, 40 parts by weight of physically modified starch, 20 parts by weight of hydroxypropyl methylcellulose, 8 parts by weight of sodium carboxymethylcellulose, 10 parts by weight of gellan gum, and 5 parts by weight of gelatin 1. Mix 2 parts by weight of chitosan with 1.5 parts by weight of sodium citrate to obtain a powdery material, then add water to the powdery material according to the weight ratio of the powdery material to water at 1:2.4, stir and mix , dissolving the powdery material to obtain a raw material mixture solution.
[0098] B. Preparation of composite gel
[0099] heating the polyethylene glycol to a temperature of 80°C to completely melt it, and then mixing the molten polyethylene glycol with ...
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