Thermally conductive fluororubber and preparation method thereof, and laser projection equipment
A fluororubber and thermally conductive filler technology, which is applied in the field of thermally conductive fluororubber and its preparation, can solve the problems of poor thermal conductivity and decreased mechanical properties of fluororubber, and achieve the effects of good processing performance, improved uniform dispersion and uniform distribution.
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[0043] A preparation method of heat-conducting fluororubber, comprising the following steps:
[0044] Step 1. Disperse the thermally conductive filler into the fluororubber matrix;
[0045] Step 2, dispersing the vulcanizing agent into the fluororubber matrix;
[0046] Step 3, making the vulcanizing agent and the fluororubber matrix undergo a crosslinking reaction to obtain a heat-conducting fluororubber;
[0047] Wherein, the thermally conductive filler is a thermally conductive filler prepared according to the following method;
[0048] Step (a): react the fluororubber monomer, excess mercaptan and photoinitiator in the first organic solvent under the condition of light to obtain the first reactant, then remove the first organic solvent and unreacted mercaptan The compound obtains a second reactant, and the second reactant is dissolved in a second organic solvent to obtain a solution of the second reactant;
[0049] Step (b): dispersing the metal powder into the solution ...
Embodiment 1
[0075] Step 1, 100 parts of fluororubber raw rubber (that is, fluororubber matrix) is plasticized for 10 minutes on an open mill with a roll distance of 5 mm, then add 10 parts of thermally conductive filler (the preparation method of thermally conductive filler is as described later ) was mixed for 15 minutes;
[0076] Step 2, adding 2 parts of bisphenol AF and 0.5 part of benzyltriphenylphosphorous chloride to the raw material after mixing;
[0077] Step 3. Thin pass pressing 6 times on an open mill with a roller distance of 1 mm, and then enlarge the roller distance to 1.5 mm to remove the sheet and park to obtain a heat-conducting fluororubber.
[0078] Preparation of thermally conductive filler
[0079] The preparation method of the thermally conductive filler in the present embodiment is as follows:
[0080] Step (a), add 100 parts of vinylidene fluoride, 2 parts of 3,6-dioxa-1,8-octanedithiol, and 2 parts of BAPO into tetrahydrofuran in sequence, stir at room temper...
Embodiment 2
[0083] Step 1, 100 parts of fluororubber raw rubber (that is, fluororubber matrix) is plasticized for 10 minutes on an open mill with a roll distance of 2 mm, and then 40 parts of thermally conductive fillers are added (the preparation method of thermally conductive fillers is as described later. ) was mixed for 20 minutes;
[0084] Step 2, adding 2.3 parts of bisphenol AF and 0.7 part of benzyltriphenylphosphorous chloride to the raw material after mixing;
[0085] Step 3. Thin pass and press 8 times on an open mill with a roller distance of 0.5 mm, and then enlarge the roller distance to 2 mm to remove the sheet and park to obtain a heat-conducting fluororubber.
[0086] Preparation of thermally conductive filler
[0087] The preparation method of the thermally conductive filler in the present embodiment is as follows:
[0088] Step (a), add 100 parts of vinylidene fluoride, 20 parts of 3,6-dioxa-1,8-octanedithiol, and 20 parts of BAPO into tetrahydrofuran in turn, stir ...
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