Method for preparing roasted fragrant and sweet components of red dates and application of roasted fragrant and sweet components of red dates to pipe tobacco
A technology for red dates and roasted sweetness is applied in the field of preparation of roasted sweet aroma components of red dates. Production application, increased sweetness, prominent effect of roasted sweetness
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Embodiment 1
[0028] ⑴ Preparation of Roasted Sweet Fragrance of Red Dates
[0029]Commercially available Xinjiang jujube (dried jujube), about 1.5 kg after being washed, pitted and sun-dried. Use 75% ethanol to heat to 60°C for extraction, the mass ratio of solid to liquid is 1:6, and extract twice for 2 hours each time. The two extracts were combined, first filtered with a 200 nm microfiltration membrane to collect the permeate, and then passed through a 5 kD ultrafiltration membrane to collect the ultrafiltration permeate. Concentrate the ultrafiltration permeate under reduced pressure to obtain 550 g without alcohol smell; at this time, add 300 g of distilled water, stir and mix well, and then put it on a D-101 macroporous adsorption resin chromatography column (the inner diameter of the column is 8 cm, and the packing height is 70 cm, with a column volume of about 3.5 L; the resin filler was purchased from Sinopharm Chemical Reagent Co., Ltd.), after standing for 6 h for adsorption, r...
Embodiment 2
[0048] Commercially available Xinzheng jujube (dried jujube) was washed, pitted, and dried at low temperature. Weighed 1 kg and extracted it with 65% ethanol in a circular ultrasonic cycle. The mass ratio of solid to liquid was 1:15. The extraction temperature was 35°C and the ultrasonic frequency was 40 kHz. The power was 750 W, the stirring speed was 1500 rpm, the extraction time was 50 min in total, and the ultrasonic time and interval time were 2 s / 1 s. The extract was filtered through a 50 nm microfiltration membrane, and then passed through a 5 kD ultrafiltration membrane to collect the ultrafiltration permeate. Concentrate the ultrafiltration permeate under reduced pressure until it has no alcohol smell to obtain 350 g of extract, add 200 g of deionized water, stir and mix well, and then put it on the AB-8 macroporous adsorption resin chromatography column (column inner diameter 6 cm, packing The height of the column is 60 cm, and the column volume is about 1.7 L; the r...
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