Device and method for separating catalyst and heavy hydrocarbons in slurry bed reactor
A separation device and catalyst technology, applied in the petrochemical field, can solve the problems of accelerating the separation of solid catalyst particles and slurry, reducing the overall performance of the catalyst, and agglomerating and agglomerating, achieving the effects of short action time, mild filtration conditions and high separation effect.
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Embodiment 1
[0049] Filter I:
[0050] Filter tank 1 has a cross-sectional diameter of 1m, a height of 3m, and a volume of 2m 3 ;The filter medium is 310μm in diameter and 0.1g / cm in density 3 The hollow iron sphere is covered with a layer of polytetrafluoroethylene material; the sieve plate 2 is located at the bottom of the filter tank 1, and the mesh diameter of the sieve plate 2 is 300 μm; the thickness of the filter medium accumulated on the sieve plate 2 is 0.05m.
[0051] Filter by:
[0052] 1. Turn on the electromagnet 3, so that the magnetic filter medium is densely and evenly piled on the sieve plate 2 in the filter tank 1, and open the valve HV-1 to introduce the slurry I into the filter tank 1;
[0053] 2. Close the valve HV-1, open the valve HV-8, so that the filtrate enters the filtrate tank 4, when the volume of the filtrate in the filtrate tank 4 reaches 0.8m 3 And the volume increase rate is less than 0.1m 3 / h, open the valve HV-4 and circulating pump 7, reintroduce th...
Embodiment 2
[0058] Filter II:
[0059] Filter tank 1 has a cross-sectional diameter of 1m, a height of 3m, and a volume of 2m 3 ;The filter medium is projected surface diameter 1000μm, density 0.5g / cm 3 A hollow cobalt tetrahedron, which is covered with a layer of polypropylene material; the sieve plate 2 is located at the bottom of the filter tank, and the mesh diameter of the sieve plate 2 is 800 μm; the thickness of the filter medium accumulated on the sieve plate 2 is 0.25m;
[0060] Filter by:
[0061] 1. Turn on the electromagnet 3, so that the magnetic filter medium is densely and evenly piled on the sieve plate 2 in the filter tank 1, and the slurry II is introduced into the filter tank 4 through the valve HV-1;
[0062] 2. Close the valve HV-1, open the valve HV-8, so that the filtrate enters the filtrate tank 4, when the volume of the filtrate in the filtrate tank 4 reaches 0.8m 3 And the volume increase rate is less than 0.1m 3 / h, open the valve HV-4 and circulation pump 7...
Embodiment 3
[0067] Filter III:
[0068] Filter tank 1 has a cross-sectional diameter of 1m, a height of 3m, and a volume of 2m 3 ;The filter medium is projected surface diameter 6000μm, density 1.1g / cm 3 The hollow nickel cube is covered with a layer of ceramic material; the sieve plate 2 is located at the bottom of the filter tank 1, and the mesh diameter of the sieve plate 2 is 4000 μm; the thickness of the filter medium accumulated on the sieve plate 2 is 0.5m.
[0069] Filter by:
[0070] 1. Turn on the electromagnet 3, so that the magnetic filter medium is evenly accumulated on the sieve plate 2 in the filter tank 1, and open the valve HV-1 to introduce the slurry III into the filter tank 1;
[0071] 2. Close the valve HV-1, open the valve HV-8, so that the filtrate enters the filtrate tank 4, when the volume of the filtrate in the filtrate tank 4 reaches 0.8m 3 And the volume increase rate is less than 0.1m 3 When / h, open valve HV-4 and circulation pump 7, filtrate is reintrodu...
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