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Device and method for separating catalyst and heavy hydrocarbons in slurry bed reactor

A separation device and catalyst technology, applied in the petrochemical field, can solve the problems of accelerating the separation of solid catalyst particles and slurry, reducing the overall performance of the catalyst, and agglomerating and agglomerating, achieving the effects of short action time, mild filtration conditions and high separation effect.

Active Publication Date: 2017-12-26
WUHAN KAIDI ENG TECH RES INST CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These two patents use magnetic force to accelerate the separation of solid catalyst particles and slurry. During the separation process, the catalyst is always in the magnetic field. The magnetic Fischer-Tropsch catalyst is easily magnetized and aggregated, reducing the overall performance of the catalyst.

Method used

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  • Device and method for separating catalyst and heavy hydrocarbons in slurry bed reactor
  • Device and method for separating catalyst and heavy hydrocarbons in slurry bed reactor
  • Device and method for separating catalyst and heavy hydrocarbons in slurry bed reactor

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0049] Filter I:

[0050] Filter tank 1 has a cross-sectional diameter of 1m, a height of 3m, and a volume of 2m 3 ;The filter medium is 310μm in diameter and 0.1g / cm in density 3 The hollow iron sphere is covered with a layer of polytetrafluoroethylene material; the sieve plate 2 is located at the bottom of the filter tank 1, and the mesh diameter of the sieve plate 2 is 300 μm; the thickness of the filter medium accumulated on the sieve plate 2 is 0.05m.

[0051] Filter by:

[0052] 1. Turn on the electromagnet 3, so that the magnetic filter medium is densely and evenly piled on the sieve plate 2 in the filter tank 1, and open the valve HV-1 to introduce the slurry I into the filter tank 1;

[0053] 2. Close the valve HV-1, open the valve HV-8, so that the filtrate enters the filtrate tank 4, when the volume of the filtrate in the filtrate tank 4 reaches 0.8m 3 And the volume increase rate is less than 0.1m 3 / h, open the valve HV-4 and circulating pump 7, reintroduce th...

Embodiment 2

[0058] Filter II:

[0059] Filter tank 1 has a cross-sectional diameter of 1m, a height of 3m, and a volume of 2m 3 ;The filter medium is projected surface diameter 1000μm, density 0.5g / cm 3 A hollow cobalt tetrahedron, which is covered with a layer of polypropylene material; the sieve plate 2 is located at the bottom of the filter tank, and the mesh diameter of the sieve plate 2 is 800 μm; the thickness of the filter medium accumulated on the sieve plate 2 is 0.25m;

[0060] Filter by:

[0061] 1. Turn on the electromagnet 3, so that the magnetic filter medium is densely and evenly piled on the sieve plate 2 in the filter tank 1, and the slurry II is introduced into the filter tank 4 through the valve HV-1;

[0062] 2. Close the valve HV-1, open the valve HV-8, so that the filtrate enters the filtrate tank 4, when the volume of the filtrate in the filtrate tank 4 reaches 0.8m 3 And the volume increase rate is less than 0.1m 3 / h, open the valve HV-4 and circulation pump 7...

Embodiment 3

[0067] Filter III:

[0068] Filter tank 1 has a cross-sectional diameter of 1m, a height of 3m, and a volume of 2m 3 ;The filter medium is projected surface diameter 6000μm, density 1.1g / cm 3 The hollow nickel cube is covered with a layer of ceramic material; the sieve plate 2 is located at the bottom of the filter tank 1, and the mesh diameter of the sieve plate 2 is 4000 μm; the thickness of the filter medium accumulated on the sieve plate 2 is 0.5m.

[0069] Filter by:

[0070] 1. Turn on the electromagnet 3, so that the magnetic filter medium is evenly accumulated on the sieve plate 2 in the filter tank 1, and open the valve HV-1 to introduce the slurry III into the filter tank 1;

[0071] 2. Close the valve HV-1, open the valve HV-8, so that the filtrate enters the filtrate tank 4, when the volume of the filtrate in the filtrate tank 4 reaches 0.8m 3 And the volume increase rate is less than 0.1m 3 When / h, open valve HV-4 and circulation pump 7, filtrate is reintrodu...

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Abstract

A separation device for a catalyst and heavy hydrocarbon in a slurry bed reactor. The separation device comprises a filter tank (1), a sieve plate (2), an electromagnet (3) and a filtrate tank (4). A catalyst outlet of the filter tank (1) is connected to an input end of the filtrate tank (4). An output end of the filtrate tank (4) is connected to a filtrate circulation return inlet of the filter tank (1). A pipeline between the output end of the filtrate tank (4) and the filtrate circulation return inlet of the filter tank (1) is communication with a product conveying pipe of a product storage tank (5). The catalyst outlet of the filter tank (1) is further connected to a catalyst discharging pipe. A lower portion inside the filter tank (1) is provided with the sieve plate (2), on which a magnetic filter medium layer (6) is provided. The filter tank (1) is provided with the electromagnet (3), which generates a uniform magnetic field at the sieve plate (2). The separation device provides highly efficient solid-liquid separation without blocking a filter medium, and a separated solid catalyst can be recycled and reused, enabling a slurry bed reactor to operate continuously in industrial applications.

Description

technical field [0001] The invention relates to the field of petrochemical technology, in particular to a device and method for separating catalysts and heavy hydrocarbons in a slurry bed reactor. Background technique [0002] Combine CO and H 2 The method of converting the synthesized gas into hydrocarbons through catalyst action was invented by German scientists Frans Fischer and Hans Tropsch in 1923, referred to as Fischer-Tropsch synthesis. The basic principle is that CO undergoes a heterogeneous catalytic hydrogenation reaction on a metal catalyst to form a mixture mainly composed of linear alkanes and alkenes. [0003] With the depletion of petroleum resources, it is a good alternative to petroleum to produce synthetic gas from various hydrocarbon-containing resources such as natural gas, coal, and biomass, and then to produce liquid fuel through Fischer-Tropsch synthesis reaction using synthetic gas as raw material. way, is being valued by more and more countries. ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J8/22C10G2/00B01D35/06
CPCB01D35/06B01J8/22C10G2/00
Inventor 汪大闪刘倩倩李昌元饶莎莎宋德臣詹晓东
Owner WUHAN KAIDI ENG TECH RES INST CO LTD
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