Water-dispersible composition comprising carotenoid crystals for imparting a red color
A carotene and crystal dispersion technology, applied in application, food science, food ingredients, etc., can solve problems such as water-dispersible compositions that do not know red oil-soluble pigment crystals, and achieve less color change, heat resistance and Excellent light fastness effect
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Embodiment 1)
[0099] (Example 1) Water-dispersible composition of β-carotene crystals using polysorbate 80 and water
[0100] Dissolve / sterilize polysorbate 80 (component C: 36g), glycerin (component E: 183g) and purified water (component D: 33g) at 90-95°C for 15 minutes, then cool to 50-55°C. Tocopherol (0.6 g) and sorbitan monooleate (B component: 6 g) were added to this mixture, and the aqueous phase was prepared. Add crystallized β-carotene (component A: 15 g) to the water phase, and stir at 6,000 to 7,000 rpm for 15 minutes using a high-speed emulsifier (TK-homomixer: manufactured by PRIMIX Co., Ltd.) to obtain crystals Crush the stock solution. 250 g of this stock solution was stirred and pulverized at 2000 rpm for 3 hours with a wet pulverizer (OB MILL 0.5 type: manufactured by Freund Turbo. Co., Ltd.) to obtain a pulverized product. Purified water (20.3 g) was added to the pulverized product (234.5 g), and stirred at 3,000 rpm for 5 minutes with a high-speed emulsifier to obtain ...
Embodiment 2)
[0101] (Example 2) Water-dispersible composition of β-carotene crystals using polyglyceryl fatty acid ester and ethanol
[0102]Decacylglycerol monooleate (component F: 36g), glycerin (component E: 183g) and ethanol (component G: 33g) were dissolved / sterilized by heating at 90-95°C for 15 minutes, then cooled to 50-55°C. Tocopherol (0.6 g) and sorbitan monooleate (B component: 6 g) were added to this mixture, and the aqueous phase was prepared. Crystallized β-carotene (15 g) was added to the water phase, and stirred at 6,000 to 7,000 rpm for 15 minutes using a high-speed emulsifier (TK-homomixer: manufactured by PRIMIX Corporation) to obtain a crystal crushed stock solution. 250 g of this stock solution was stirred and pulverized at 2000 rpm for 3 hours with a wet pulverizer (OB MILL 0.5 type: manufactured by Freund Turbo. Co., Ltd.) to obtain a pulverized product. Purified water (22.5 g) was added to the treated product (228 g), and stirred at 3,000 rpm for 5 minutes with a ...
Embodiment 3)
[0127] (Example 3) Water-dispersible composition of β-carotene crystals using polysorbate 20 and water
[0128] Except having used the polysorbate 20 instead of the polysorbate 80 of Example 1, it carried out completely the same operation as Example 1, and obtained this invention product 3 (240g).
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