Intelligent gel particles capable of being crosslinked again under stratum condition and preparation method and application of intelligent gel particles
A technology of cross-linking gel and smart gel is applied to smart gel particles and the preparation method and application field thereof, which can solve the problems of reduced mechanical strength, influence of precipitation effect, easy breakage and the like, and achieves the effect of improving erosion resistance.
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Embodiment 1
[0057] Embodiment 1, a kind of recrosslinkable intelligent gel particle, the mass percent of raw material composition is as follows:
[0058] Acrylamide 30%, 2-acrylamido-2-methylpropanesulfonic acid (AMPS) 10%, methacryloyloxyethyltrimethylammonium chloride 5%, N,N-vinylpyrrolidone 3%, Azobisisobutyronitrile 0.15%, appropriate amount of sodium hydroxide, N,N-methylenebisacryloyl 0.1%, n-butyl titanate 0.1%, EDTA 0.1%, nano-bentonite (500nm) 3.5%, balance for water.
[0059] The preparation method is as follows:
[0060] Introduce nitrogen into deionized water for 30 minutes, then add 3.5% nano-bentonite, disperse ultrasonically for 30 minutes with an ultrasonic cleaner (300W) at room temperature, add 30% acrylamide, 5% methacryloyloxyethyltrimethylammonium chloride , N,N-vinylpyrrolidone 3%, after stirring and dissolving completely, adjust the pH value of the solution to 7.0-8.5 with 25% aqueous sodium hydroxide solution, then add 0.1% EDTA and 0.15% azobisisobutyronitrile ...
Embodiment 2
[0062] As described in Example 1, the difference is that the mass percentage of nano-bentonite is 8%.
Embodiment 3
[0064] As described in Example 1, the difference is that the mass percentage of nano-bentonite is 0%.
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