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Modified graphene-coated lithium nickelate positive electrode material of battery and preparation method thereof

A graphene-coated, cathode material technology, applied in battery electrodes, circuits, electrical components, etc., can solve problems such as restricting development prospects, lack of nickel resources, toxicity, etc., to prolong storage time, improve self-discharge, and the method is simple Effect

Inactive Publication Date: 2016-03-16
王晓伟
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  • Abstract
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  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Since the commercialization of lithium-ion batteries, most of the positive electrode materials used in lithium-ion batteries are lithium nickelate, lithium nickelate or ternary materials, etc., and its components are mainly active materials plus conductive agents and then binders. The active materials It is lithium nickelate, lithium nickelate or ternary, etc.; most of the negative electrode materials use graphite as the active material, and then add some conductive agent and binder; its advantages are high capacity and long cycle life, but nickel resources are scarce and expensive And it is toxic, so it is an important research direction for lithium-ion batteries to seek cheap, reliable, and environmentally friendly cathode materials.
Spinel-type positive electrode materials represented by lithium nickel oxide and layered oxides of ternary materials have been extensively studied in the past decade, but their development prospects are restricted by their respective defects.

Method used

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Embodiment Construction

[0011] The modified graphene-coated lithium nickelate battery positive electrode material is prepared in parts by weight from the following components in the proportions shown: graphene oxide 50, lithium nickelate 40, 45% lithium iron nitrate solution 30, flakes Graphite 8, bonding material 8.

[0012] The preparation method of the modified graphene-coated lithium nickelate battery cathode material comprises the following steps:

[0013] (1) get graphite and sodium nitrate, with mass ratio 2:1 ratio, place in the vitriol oil of a certain amount of ice bath, add 3 times of potassium high nickelate of described graphite quality under stirring, mix homogeneously, control temperature is low Stir at 20°C for about 1 hour, then raise the temperature to 32-38°C for 2 hours, slowly add quantitative deionized water dropwise, stir well, add hydrogen peroxide to stop the reaction when the temperature of the system drops, filter, wash, and dry; heat and stir In the process of adding a ce...

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Abstract

The invention relates to a modified graphene-coated lithium nickelate positive electrode material of a battery and a preparation method thereof. The modified graphene-coated lithium nickelate positive electrode material is prepared from the following components by weight: 50 parts of graphene oxide, 40 parts of lithium nickelate, 30 parts of a lithium ferric nitrate solution with a concentration of 45%, 8 parts of flake graphite and 8 parts of a bonding material. The modified graphene-coated lithium nickelate positive electrode material overcomes the defect of failure caused by self-discharging of a protection plate of a lithium ion battery, so self-discharging of a whole battery pack is improved, the purpose of prolongation of the storage time of the lithium battery is achieved, and it is guaranteed that the lithium battery can be stored for a long time under the condition that a user does not charge an electric appliance after usage.

Description

technical field [0001] The invention relates to a modified graphene-coated lithium nickelate battery positive electrode material and a preparation method thereof. Background technique [0002] Since the commercialization of lithium-ion batteries, most of the cathode materials used in lithium-ion batteries are lithium nickelate, lithium nickelate or ternary materials, etc., and its components are mainly active materials plus conductive agents and binders. Lithium nickelate, lithium nickelate or ternary, etc.; most of the negative electrode materials use graphite as the active material, and then add some conductive agents and binders; its advantages are high capacity and long cycle life, but nickel resources are scarce and expensive. And it is toxic, so it has become an important research direction for lithium-ion batteries to seek cathode materials that are inexpensive, reliable, and environmentally friendly. Spinel-type cathode materials and ternary material layered oxides,...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01M4/36H01M4/525H01M4/62H01M10/0525
CPCH01M4/366H01M4/525H01M4/625H01M10/0525Y02E60/10
Inventor 王晓伟
Owner 王晓伟
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