Preparation method for micro-capsulate type sustained-release bird repellent mixture
A microcapsule, slow-release technology, applied in botanical equipment and methods, pest repellants, animal repellents, etc., can solve the problems of high cost, low efficiency, poor weather resistance, etc., and achieve good weather resistance and service life. Long, bird repellent effect
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Embodiment 1
[0023] In a 1000ml three-necked flask equipped with a mechanical stirrer, a heating device, and a condensing reflux device, add 200 g of deionized water and 50 g of 2.5 wt % maleic anhydride, 4.8 g of urea, 0.5 g of ammonium chloride, and 0.5 g of resorcinol Phenol was stirred and dissolved evenly. Add 5g of musk-T, 20g of cinnamic amide, and 2g of ethyl hydroxybenzoate mixture slowly dropwise into the flask to form an emulsion; then add 11.28g of 37% formaldehyde solution (formalin), slowly heat up to 56°C for 4 hours, cool Washing with water for 5 times, vacuum drying to obtain the microcapsule product with the effect of promoting bird repelling.
Embodiment 2
[0025] In a 1000ml three-necked flask equipped with a mechanical stirrer, a heating device, and a condensing reflux device, add 350g of deionized water and 75g of 1wt% maleic anhydride, 20g of urea, 4g of ammonium chloride, and 3.6g of resorcinol and stir to dissolve evenly . Slowly drop the mixture of 60g musk-T, 75g cinnamic acid and 5g benzoic acid into the flask to form an emulsion; then add 30g 37% formaldehyde solution (formalin), slowly raise the temperature to 60°C for 4 hours, wash with cooling water for 3-5 Second, vacuum drying to obtain a microcapsule product with the effect of promoting bird avoidance.
Embodiment 3
[0027] In a 1000ml three-necked flask equipped with a mechanical stirrer, a heating device, and a condensing reflux device, add 250 g of deionized water and 40 g of 5 wt % maleic anhydride, 4 g of urea, 0.5 g of ammonium chloride, and 0.6 g of resorcinol and stir to dissolve uniform. Slowly drop a mixture of 5g musk-T, 25g cinnamic acid, and 2.5g benzoic acid into the flask to form an emulsion; then add 10g of 37% formaldehyde solution (formalin), slowly raise the temperature to 50°C for 3 hours, and wash with cooling water for 3~ 5 times, vacuum-dried to obtain a microcapsule product with the effect of promoting bird avoidance.
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