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Circulating filtration type nuclear pore membrane etching device

A circulating filtration and etching device technology, applied in the preparation of test samples, etc., can solve problems such as film rolling machine transmission failure, etching solution concentration changes, etching speed changes, etc., to ensure temperature control accuracy, liquid preparation operation is convenient, The effect of improving the uniformity of temperature and concentration

Active Publication Date: 2016-01-27
INST OF MODERN PHYSICS CHINESE ACADEMY OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] (1) The nuclear pore membrane is not cleaned after etching, and there is alkaline residue
[0005] (2) During the etching process, due to the volatilization of the etching solution and other reasons, the concentration of the etching solution changes, resulting in a change in the etching rate, resulting in uneven pore size of the nuclear pore membrane
[0006] (3) The etching tank is generally heated by a heater, and the temperature changes in different areas, and the etching rate is different in different etching positions, resulting in uneven etching
[0007] (4) During the etching process, residues will be produced due to the reaction between the membrane and the etching solution, which will cause the transmission failure of the film rolling machine; at the same time, the etching solution will become turbid and adhere to the surface of the nuclear pore membrane to hinder the etching of the nuclear pore membrane, resulting in uneven etching pore size
[0009] At present, these problems still plague the etching process of nuclear pore membranes and affect the product quality of nuclear pore membranes.

Method used

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  • Circulating filtration type nuclear pore membrane etching device
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Examples

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Effect test

Embodiment 1

[0025] Example 1: see figure 1 , a circulating filter type nuclear pore membrane etching device. The device mainly includes a liquid distribution tank 1, an etching tank 2, a heating tank 3, and a liquid replacement tank 4. The pipeline of etching tank 2 is connected to the input port of heating tank 3, and the pipeline is provided with waterway switch 3.1; the output of heating tank 3 is connected to etching tank 2 through circulating filter 3.3, and heater 3.2 is arranged in heating tank 3, and heater 3.2 monitors etching The thermal probe 3.4 of the liquid temperature is arranged in the etching tank 2; the agitator 1.1 is arranged in the liquid distribution tank 1, and the liquid distribution tank 1 is connected to the etching tank 2 through the water circuit switch 1.1 and the liquid adding filter 1.2; There is a concentration probe 4.1 for monitoring the concentration in the heating tank 3, and the replenishment tank automatically supplies etching solution to the etching...

Embodiment 2

[0026] Example 2: see figure 2 , a circulating filter type nuclear pore membrane etching device. The film transmission mechanism includes an unwinder 5, an etching tank 2, a cleaning machine 6, a dryer 7 and a winder 8 which are arranged in sequence, and the unwinder 1 is provided with an unwinding reel 1.1 of the nuclear pore membrane; The etching tank 2 is provided with an etching pressure roller 2.1 for transporting the nuclear pore membrane, and the cleaning machine 3 is provided with a cleaning pressure roller 6.1 for conveying the nuclear pore membrane; the drying machine 7 is provided with a drying pressure roller for conveying the nuclear pore membrane 7.1; The winding press roller 8.1 of the nuclear pore membrane is provided on the winding machine 8 . The cleaning machine 6 is sequentially provided with an acid-base neutralization tank 6.2, a first washing tank 6.3, a second washing tank 6.4 and an ultrasonic cleaning tank 6.5 which are not connected to each other. ...

Embodiment 3

[0035] Embodiment 3: see figure 1 and figure 2 , a circulating filter type nuclear pore membrane etching device. The device mainly includes a film etching mechanism and a film driving mechanism. The film etching mechanism includes a liquid distribution tank 1 , an etching tank 2 , a heating tank 3 and a liquid replenishing tank 4 . The pipeline of etching tank 2 is connected to the input port of heating tank 3, and the pipeline is provided with waterway switch 3.1; the output of heating tank 3 is connected to etching tank 2 through circulating filter 3.3, and heater 3.2 is arranged in heating tank 3, and heater 3.2 monitors etching The thermal probe 3.4 of the liquid temperature is arranged in the etching tank 2; the agitator 1.1 is arranged in the liquid distribution tank 1, and the liquid distribution tank 1 is connected to the etching tank 2 through the water circuit switch 1.1 and the liquid adding filter 1.2; There is a concentration probe 4.1 for monitoring the conce...

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Abstract

The invention discloses a circulating filtration type nuclear pore membrane etching device. The device is used for nuclear pore membrane batch etching machining and mainly applied to the fields of nuclear pore membrane product machining, nuclear pore membrane preparation and the like. The circulating filtration type nuclear pore membrane etching device is mainly characterized in that an etching groove is connected with an input port of a heating groove through a pipeline, and the pipeline is provided with a water path switch; output of the heating groove is connected with the etching groove through a circulating filtration machine, heaters are arranged in the heating groove, and a thermosensitive probe for monitoring the temperature of etching liquid for the heaters is arranged in the etching groove; a stirrer is arranged in a liquid blending groove, and the liquid blending groove is connected with the etching groove through a water path switch and a liquid addition filtration machine via a pipeline; a concentration probe for monitoring concentration in the heating groove is arranged in a liquid supply groove, and the liquid supplement groove supplies etching liquid to the etching groove automatically. The device has the advantages of automatic temperature and concentration compensation, circulating flow, self-cleaning performance and the like, and can perform nuclear pore membrane batch etching efficiently for a long time.

Description

technical field [0001] The invention relates to a batch etching device for nuclear pore membranes. This device is mainly used for batch etching processing of nuclear pore membranes, and its main application fields include nuclear pore membrane product processing, nuclear pore membrane preparation, etc. Background technique [0002] Nuclear pore membrane, also known as nuclear microporous membrane or heavy ion microporous membrane, is formed by punching holes in the insulating material film with heavy ions and then chemically etching to expand the pores. The etching process is mainly to immerse the irradiated membrane material in an alkaline etching liquid. Alkaline liquid generally adopts 2-8 mol / liter sodium hydroxide solution, and the etching temperature is generally 50-80°C. Since the pore diameter of the nuclear pore membrane is proportional to the etching time under the same etching conditions, nuclear pore membranes with different pore diameters are usually produced ...

Claims

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Application Information

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IPC IPC(8): G01N1/32
Inventor 莫丹袁平刘杰梁伟张瑞庆李运杰曹殿亮
Owner INST OF MODERN PHYSICS CHINESE ACADEMY OF SCI
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